benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--4-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside

Base Information

Chemical Name:benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--4-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside
CAS No.:74221-01-5
Molecular Formula:C₂₅H₃₇NO₁₁S
Molecular Weight:559.635
Hs Code.:

benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O-<D-1-(methoxycarbonyl)ethyl>-4-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside

Synonyms:benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--4-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside

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Chemical Property of benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--4-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside

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Technology Process of benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--4-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside

There total 4 articles about benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--4-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 110-87-2
3,4-dihydro-2H-pyran

: 74221-00-4
benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--α-D-glucopyranoside

: 74221-01-5
benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--4-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside

Guidance literature:: With toluene-4-sulfonic acid; In 1,4-dioxane; for 2.5h; Ambient temperature;
DOI:10.1080/00021369.1980.10864112

Reference yield:

: 40269-09-8
benzyl 2-acetamido-2-deoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-α-D-glucopyranoside

: 74221-01-5
benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--4-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / pyridine / 5 h / -20 °C

2: 99 percent / p-toluenesulfonic acid monohydrate / dioxane / 2.5 h / Ambient temperature

With pyridine; toluene-4-sulfonic acid; In 1,4-dioxane;
DOI:10.1080/00021369.1980.10864112

Reference yield:

: 69323-67-7
(R)-2-(((4aR,6S,7R,8R,8aS)-7-acetamido-6-(benzyloxy)-2,2-dimethylhexahydropyrano[3,2-d][1,3]dioxin-8-yl)oxy)propanoic acid

: 74221-01-5
benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--4-O-(tetrahydropyran-2-yl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: Amberlite IR 120(H⁽¹⁺⁾) resin / Heating

2: 85 percent

With Amberlite IR 120(H⁽¹⁺⁾) resin;
DOI:10.1016/S0008-6215(00)85146-0