3,5-Dimethoxy-4,6-dimethyl-(6R)-6-((2R)-2-methylbutyryloxy)cyclohexa-2,4-dien-1-one

Base Information

• Chemical Name: 3,5-Dimethoxy-4,6-dimethyl-(6R)-6-((2R)-2-methylbutyryloxy)cyclohexa-2,4-dien-1-one
• CAS No.: 107811-68-7
• Molecular Formula: C₁₅H₂₂O₅
• Molecular Weight: 282.337

Synonyms:3,5-Dimethoxy-4,6-dimethyl-(6R)-6-((2R)-2-methylbutyryloxy)cyclohexa-2,4-dien-1-one

Chemical Property of 3,5-Dimethoxy-4,6-dimethyl-(6R)-6-((2R)-2-methylbutyryloxy)cyclohexa-2,4-dien-1-one

Chemical Property:

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Technology Process of 3,5-Dimethoxy-4,6-dimethyl-(6R)-6-((2R)-2-methylbutyryloxy)cyclohexa-2,4-dien-1-one

There total 2 articles about 3,5-Dimethoxy-4,6-dimethyl-(6R)-6-((2R)-2-methylbutyryloxy)cyclohexa-2,4-dien-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.8%

diazomethane (186581-53-3,908094-01-9,334-88-3) + 4,5-Dimethyl-5-methoxy-(4S)-4-(2-methylbutyryloxy)cyclohex-5-ene-1,3-dione → 3,5-Dimethoxy-4,6-dimethyl-(6R)-6-((2R)-2-methylbutyryloxy)cyclohexa-2,4-dien-1-one (107811-68-7) + 2,4-Dimethyl-3,5-dimethoxy-(4S)-4-((2R)-2-methylbutyryloxy)cyclohexa-2,5-diene-1-one + 2,4-Dimethyl-3,5-dimethoxy-(4S)-4-((2S)-2-methylbutyryloxy)cyclohexa-2,5-diene-1-one

Guidance literature:

In diethyl ether; ethyl acetate; Yield given;

DOI:10.1055/s-1998-2083

Reference yield: 31.8%

diazomethane (186581-53-3,908094-01-9,334-88-3) + 4,5-Dimethyl-5-methoxy-(4S)-4-(2-methylbutyryloxy)cyclohex-5-ene-1,3-dione → 3,5-Dimethoxy-4,6-dimethyl-(6R)-6-((2R)-2-methylbutyryloxy)cyclohexa-2,4-dien-1-one (107811-68-7) + 3,5-Dimethoxy-4,6-dimethyl-(6R)-6-((2S)-2-methylbutyryloxy)cyclohexa-2,4-dien-1-one + 2,4-Dimethyl-3,5-dimethoxy-(4S)-4-((2R)-2-methylbutyryloxy)cyclohexa-2,5-diene-1-one + 2,4-Dimethyl-3,5-dimethoxy-(4S)-4-((2S)-2-methylbutyryloxy)cyclohexa-2,5-diene-1-one

Guidance literature:

In diethyl ether; ethyl acetate; Yields of byproduct given;

DOI:10.1055/s-1998-2083

Reference yield: 69.0%

3,5-Dimethoxy-4,6-dimethyl-(6R)-6-((2R)-2-methylbutyryloxy)cyclohexa-2,4-dien-1-one (107811-68-7) → (R)-2-Methyl-butyric acid (S)-2-hydroxy-4-methoxy-1,3-dimethyl-6-oxo-cyclohexa-2,4-dienyl ester (90129-40-1)

Guidance literature:

With aluminium trichloride; ethanethiol; In dichloromethane; for 18h; Ambient temperature;

DOI:10.1055/s-1998-2083

upstream raw materials:

diazomethane

Downstream raw materials:

(R)-2-Methyl-butyric acid (S)-2-hydroxy-4-methoxy-1,3-dimethyl-6-oxo-cyclohexa-2,4-dienyl ester

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