Technology Process of C16H17NO5
There total 7 articles about C16H17NO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
manganese(IV) oxide;
In
dichloromethane;
at 20 ℃;
for 10h;
Inert atmosphere;
DOI:10.1021/ol202895u
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene; copper dichloride / acetonitrile / 11 h / 0 - 20 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1.5 h / -10 °C / Inert atmosphere
4: manganese(IV) oxide / dichloromethane / 10 h / 20 °C / Inert atmosphere
With
manganese(IV) oxide; tetrabutyl ammonium fluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; 3-chloro-benzenecarboperoxoic acid; copper dichloride;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/ol202895u
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1.5 h / -10 °C / Inert atmosphere
3: manganese(IV) oxide / dichloromethane / 10 h / 20 °C / Inert atmosphere
With
manganese(IV) oxide; tetrabutyl ammonium fluoride; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ol202895u
