Hexyl 2-acetamido-3-O-benzoyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:Hexyl 2-acetamido-3-O-benzoyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside
CAS No.:172945-28-7
Molecular Formula:C₂₈H₃₅NO₇
Molecular Weight:497.588
Hs Code.:

Synonyms:Hexyl 2-acetamido-3-O-benzoyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

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Chemical Property of Hexyl 2-acetamido-3-O-benzoyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

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Technology Process of Hexyl 2-acetamido-3-O-benzoyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

There total 4 articles about Hexyl 2-acetamido-3-O-benzoyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 98-88-4
benzoyl chloride

: 172945-27-6
Hexyl 2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

: 172945-28-7
Hexyl 2-acetamido-3-O-benzoyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Guidance literature:: With pyridine; for 2h;
DOI:10.1002/recl.19951140905

Reference yield:

: 10378-06-0,20757-53-3,35954-65-5,123483-77-2,134308-33-1
2-methyl-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyranoso)[1,2-d]-2-oxazoline

: 172945-28-7
Hexyl 2-acetamido-3-O-benzoyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / TfOH / CH₂Cl₂ / 2 h

2: NaOMe / methanol / 2 h

3: p-TsOH / dimethylformamide / 4 h

4: 91 percent / pyridine / 2 h

With pyridine; trifluorormethanesulfonic acid; sodium methylate; toluene-4-sulfonic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/recl.19951140905

Reference yield:

: 172945-26-5
1-hexyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

: 172945-28-7
Hexyl 2-acetamido-3-O-benzoyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: NaOMe / methanol / 2 h

2: p-TsOH / dimethylformamide / 4 h

3: 91 percent / pyridine / 2 h

With pyridine; sodium methylate; toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/recl.19951140905