10-(4-(dodecyloxy)phenyl)-3-((E)-2-(10-(4-(dodecyloxy)-phenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

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Chemical Name:10-(4-(dodecyloxy)phenyl)-3-((E)-2-(10-(4-(dodecyloxy)-phenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine
CAS No.:1357304-49-4
Molecular Formula:C₇₄H₉₆B₂N₂O₆S₂
Molecular Weight:1195.34
Hs Code.:

10-(4-(dodecyloxy)phenyl)-3-((E)-2-(10-(4-(dodecyloxy)-phenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

Synonyms:10-(4-(dodecyloxy)phenyl)-3-((E)-2-(10-(4-(dodecyloxy)-phenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

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Chemical Property of 10-(4-(dodecyloxy)phenyl)-3-((E)-2-(10-(4-(dodecyloxy)-phenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

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Technology Process of 10-(4-(dodecyloxy)phenyl)-3-((E)-2-(10-(4-(dodecyloxy)-phenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

There total 6 articles about 10-(4-(dodecyloxy)phenyl)-3-((E)-2-(10-(4-(dodecyloxy)-phenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1263170-73-5
C₆₂H₇₂Br₂N₂O₂S₂

: 1357304-49-4
10-(4-(dodecyloxy)phenyl)-3-((E)-2-(10-(4-(dodecyloxy)-phenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

Guidance literature:: C₆₂H₇₂Br₂N₂O₂S₂; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 2h;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 13h;
DOI:10.1002/pola.25074

Reference yield:

: 92-84-2
10H-phenothiazine

: 1357304-49-4
10-(4-(dodecyloxy)phenyl)-3-((E)-2-(10-(4-(dodecyloxy)-phenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

Guidance literature:: Multi-step reaction with 5 steps

1.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate

2.1: trichlorophosphate

3.1: N-Bromosuccinimide / chloroform; acetic acid

4.1: titanium tetrachloride; zinc

5.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C

5.2: 13 h / -78 - 20 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Bromosuccinimide; n-butyllithium; titanium tetrachloride; sodium t-butanolate; zinc; trichlorophosphate; In tetrahydrofuran; hexane; chloroform; acetic acid;
DOI:10.1002/pola.25074

Reference yield:

: 1263170-71-3
10-(4-dodecyloxyphenyl)-10H-phenothiazine-3-carbaldehyde

: 1357304-49-4
10-(4-(dodecyloxy)phenyl)-3-((E)-2-(10-(4-(dodecyloxy)-phenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide / chloroform; acetic acid

2.1: titanium tetrachloride; zinc

3.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C

3.2: 13 h / -78 - 20 °C

With N-Bromosuccinimide; n-butyllithium; titanium tetrachloride; zinc; In tetrahydrofuran; hexane; chloroform; acetic acid;
DOI:10.1002/pola.25074