3',5'-di-O-acetyl-2'-O-(4-methoxytetrahydropyran-4-yl)-N²-tritylguanosine

Base Information

Chemical Name:3',5'-di-O-acetyl-2'-O-(4-methoxytetrahydropyran-4-yl)-N²-tritylguanosine
CAS No.:69471-63-2
Molecular Formula:C₃₉H₄₁N₅O₉
Molecular Weight:723.783
Hs Code.:

3',5'-di-O-acetyl-2'-O-(4-methoxytetrahydropyran-4-yl)-N<sup>2</sup>-tritylguanosine

Synonyms:3',5'-di-O-acetyl-2'-O-(4-methoxytetrahydropyran-4-yl)-N²-tritylguanosine

Suppliers and Price of 3',5'-di-O-acetyl-2'-O-(4-methoxytetrahydropyran-4-yl)-N²-tritylguanosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3',5'-di-O-acetyl-2'-O-(4-methoxytetrahydropyran-4-yl)-N²-tritylguanosine

Chemical Property:

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Technology Process of 3',5'-di-O-acetyl-2'-O-(4-methoxytetrahydropyran-4-yl)-N²-tritylguanosine

There total 4 articles about 3',5'-di-O-acetyl-2'-O-(4-methoxytetrahydropyran-4-yl)-N²-tritylguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66781-55-3
3',5'-di-O-acetyl-N²-benzoylguanosine

: 69471-63-2
3',5'-di-O-acetyl-2'-O-(4-methoxytetrahydropyran-4-yl)-N²-tritylguanosine

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / p-TsOH / dioxane / 3 h

2: 76 percent / butylamine / methanol / 24 h / Ambient temperature

3: 90 percent / pyridine / 2 h / 60 °C

4: pyridine / 6 h / 80 °C

With pyridine; toluene-4-sulfonic acid; N-butylamine; In 1,4-dioxane; methanol;
DOI:10.1246/bcsj.55.2949

Reference yield:

: 17327-22-9
4-methoxy-2,6-dihydropyran

: 69471-63-2
3',5'-di-O-acetyl-2'-O-(4-methoxytetrahydropyran-4-yl)-N²-tritylguanosine

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / p-TsOH / dioxane / 3 h

2: 76 percent / butylamine / methanol / 24 h / Ambient temperature

3: 90 percent / pyridine / 2 h / 60 °C

4: pyridine / 6 h / 80 °C

With pyridine; toluene-4-sulfonic acid; N-butylamine; In 1,4-dioxane; methanol;
DOI:10.1246/bcsj.55.2949

Reference yield:

: 83906-43-8
3',5'-di-O-acetyl-2'-O-(4-methoxytetrahydropyran-4-yl)-N²-benzoylguanosine

: 69471-63-2
3',5'-di-O-acetyl-2'-O-(4-methoxytetrahydropyran-4-yl)-N²-tritylguanosine

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / butylamine / methanol / 24 h / Ambient temperature

2: 90 percent / pyridine / 2 h / 60 °C

3: pyridine / 6 h / 80 °C

With pyridine; N-butylamine; In methanol;
DOI:10.1246/bcsj.55.2949