Technology Process of C45H41N5O4
There total 6 articles about C45H41N5O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 10h;
Inert atmosphere;
DOI:10.1016/j.tetasy.2013.03.005
- Guidance literature:
-
Multi-step reaction with 5 steps
1: ethyl acetate / 20 °C / Cooling with ice; Inert atmosphere
2: trifluoroacetic acid / dichloromethane / Inert atmosphere
3: methanol / Reflux; Inert atmosphere
4: zinc; methanesulfonic acid / N,N-dimethyl-formamide / 10.5 h / -35 - 0 °C / Inert atmosphere
5: potassium carbonate / N,N-dimethyl-formamide / 10 h / 20 °C / Inert atmosphere
With
methanesulfonic acid; potassium carbonate; trifluoroacetic acid; zinc;
In
methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2013.03.005
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium hydroxide / isopropyl alcohol
2: ethyl acetate / 20 °C / Cooling with ice; Inert atmosphere
3: trifluoroacetic acid / dichloromethane / Inert atmosphere
4: methanol / Reflux; Inert atmosphere
5: zinc; methanesulfonic acid / N,N-dimethyl-formamide / 10.5 h / -35 - 0 °C / Inert atmosphere
6: potassium carbonate / N,N-dimethyl-formamide / 10 h / 20 °C / Inert atmosphere
With
methanesulfonic acid; potassium carbonate; trifluoroacetic acid; sodium hydroxide; zinc;
In
methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1016/j.tetasy.2013.03.005
