Technology Process of C55H81NO19S
There total 10 articles about C55H81NO19S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 90 percent / pyridinium p-toluenesulfonate / acetonitrile; H2O / 17 h / 68 °C
2: 82 percent / N-methylmorpholine N-oxide monohydrate; OsO4 / acetone; 2-methyl-propan-2-ol; H2O / 4 h / 20 °C
3: diisopropylethylamine; (dimethylamino)pyridine / CH2Cl2 / 17 h / -10 °C
4: 99 percent / Dess-Martin periodinane / CH2Cl2 / 14 h / 0 °C
5: 100 percent / pyridine / 18 h / 0 °C
With
pyridine; dmap; osmium(VIII) oxide; pyridinium p-toluenesulfonate; Dess-Martin periodane; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; water; acetone; acetonitrile; tert-butyl alcohol;
4: Dess-Martin oxidation;
DOI:10.1021/jm051157a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 82 percent / N-methylmorpholine N-oxide monohydrate; OsO4 / acetone; 2-methyl-propan-2-ol; H2O / 4 h / 20 °C
2: diisopropylethylamine; (dimethylamino)pyridine / CH2Cl2 / 17 h / -10 °C
3: 99 percent / Dess-Martin periodinane / CH2Cl2 / 14 h / 0 °C
4: 100 percent / pyridine / 18 h / 0 °C
With
pyridine; dmap; osmium(VIII) oxide; Dess-Martin periodane; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; water; acetone; tert-butyl alcohol;
3: Dess-Martin oxidation;
DOI:10.1021/jm051157a
