Technology Process of N1,N10-dicyclohexyl-N1,N5,N10-tris(2,3-dihydroxybenzoyl)-1,5,10-triazadecane
There total 4 articles about N1,N10-dicyclohexyl-N1,N5,N10-tris(2,3-dihydroxybenzoyl)-1,5,10-triazadecane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
boron tribromide;
In
tetrachloromethane; dichloromethane;
Ambient temperature;
DOI:10.1021/jo00338a042
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1) H2, 2) conc. HCl / 1) 95percent EtOH, 20 to 25 deg C, 1 to 3 atm, 72 h
2: 98 percent / NEt3 / tetrahydrofuran / 60 °C
3: 60 percent / BBr3 / CCl4; CH2Cl2 / Ambient temperature
With
hydrogenchloride; hydrogen; boron tribromide; triethylamine;
In
tetrahydrofuran; tetrachloromethane; dichloromethane;
DOI:10.1021/jo00338a042
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1) H2, 2) conc. HCl / 1) 95percent EtOH, 20 to 25 deg C, 1 to 3 atm, 72 h
2: 98 percent / NEt3 / tetrahydrofuran / 60 °C
3: 60 percent / BBr3 / CCl4; CH2Cl2 / Ambient temperature
With
hydrogenchloride; hydrogen; boron tribromide; triethylamine;
In
tetrahydrofuran; tetrachloromethane; dichloromethane;
DOI:10.1021/jo00338a042