(Z)-tert-butyldiphenyl((6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hex-5-en-1-yl)oxy)silane

Base Information

Chemical Name:(Z)-tert-butyldiphenyl((6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hex-5-en-1-yl)oxy)silane
CAS No.:1435478-83-3
Molecular Formula:C₂₈H₄₁BO₃Si
Molecular Weight:464.528
Hs Code.:

Synonyms:(Z)-tert-butyldiphenyl((6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hex-5-en-1-yl)oxy)silane

Suppliers and Price of (Z)-tert-butyldiphenyl((6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hex-5-en-1-yl)oxy)silane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (Z)-tert-butyldiphenyl((6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hex-5-en-1-yl)oxy)silane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (Z)-tert-butyldiphenyl((6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hex-5-en-1-yl)oxy)silane

There total 1 articles about (Z)-tert-butyldiphenyl((6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hex-5-en-1-yl)oxy)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 128217-23-2
1-(tert-butyldiphenylsilyloxy)-5-hexyne

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1435478-83-3
(Z)-tert-butyldiphenyl((6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hex-5-en-1-yl)oxy)silane

: 1435479-20-1
(E)-tert-butyldiphenyl((6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hex-5-en-1-yl)oxy)silane

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; triethylamine; tricyclohexylphosphine; In cyclohexane; at 20 ℃; for 4h; Overall yield = 62 %; Overall yield = 110 mg;
DOI:10.1039/c3ob40131f

Reference yield: 94.0%

: 1207069-39-3
C₂₆H₃₇IO₆

: 1435478-83-3
(Z)-tert-butyldiphenyl((6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hex-5-en-1-yl)oxy)silane

: 1435478-85-5
C₄₈H₆₆O₇Si

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triphenyl-arsane; silver(l) oxide; In tetrahydrofuran; water; at 20 ℃; for 0.5h;
DOI:10.1039/c3ob40131f

Reference yield:

: 1435478-83-3
(Z)-tert-butyldiphenyl((6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hex-5-en-1-yl)oxy)silane

: C₃₃H₄₉BO₃Si

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether; dibutyl ether / 0.25 h / 0 - 20 °C / Inert atmosphere; Sealed tube

2: potassium trifluoromethansulfonate; C₅₆H₅₈FeN₂O₄P₂; palladium diacetate / tetrahydrofuran / 15 h / 55 °C / Inert atmosphere; Sealed tube

With palladium diacetate; C₅₆H₅₈FeN₂O₄P₂; potassium trifluoromethansulfonate; In tetrahydrofuran; diethyl ether; dibutyl ether;
DOI:10.1002/anie.202001580