7,16-bis<4-(1-oxo-2-phenylselenylpropyl)phenyl>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Base Information

Chemical Name:7,16-bis<4-(1-oxo-2-phenylselenylpropyl)phenyl>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane
CAS No.:226936-34-1
Molecular Formula:C₄₂H₅₀N₂O₆Se₂
Molecular Weight:836.789
Hs Code.:

Synonyms:7,16-bis<4-(1-oxo-2-phenylselenylpropyl)phenyl>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

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Chemical Property of 7,16-bis<4-(1-oxo-2-phenylselenylpropyl)phenyl>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

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Technology Process of 7,16-bis<4-(1-oxo-2-phenylselenylpropyl)phenyl>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

There total 3 articles about 7,16-bis<4-(1-oxo-2-phenylselenylpropyl)phenyl>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 456-03-1
1-(4-fluorophenyl)propan-1-one

: 226936-34-1
7,16-bis<4-(1-oxo-2-phenylselenylpropyl)phenyl>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 28 percent / tetrabutylammonium fluoride trihydrate / 12 h / 150 °C

2: 1.) LDA / 1) THF, heptane, -78 deg C, 1 h; 2) THF, heptane, 0 deg C, 2 h

With tetrabutyl ammonium fluoride; lithium diisopropyl amide;
DOI:10.1016/S0040-4020(99)00167-2

Reference yield:

: 23978-55-4
1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

: 226936-34-1
7,16-bis<4-(1-oxo-2-phenylselenylpropyl)phenyl>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 28 percent / tetrabutylammonium fluoride trihydrate / 12 h / 150 °C

2: 1.) LDA / 1) THF, heptane, -78 deg C, 1 h; 2) THF, heptane, 0 deg C, 2 h

With tetrabutyl ammonium fluoride; lithium diisopropyl amide;
DOI:10.1016/S0040-4020(99)00167-2

Reference yield:

: 5707-04-0
Phenylselenyl chloride

: 226936-28-3
7,16-bis<4-(1-oxopropyl)phenyl>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

: 226936-34-1
7,16-bis<4-(1-oxo-2-phenylselenylpropyl)phenyl>-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Guidance literature:: With lithium diisopropyl amide; Yield given; Multistep reaction; 1) THF, heptane, -78 deg C, 1 h; 2) THF, heptane, 0 deg C, 2 h;
DOI:10.1016/S0040-4020(99)00167-2