2-(2-hydroxymethyl-3,4-dimethoxyphenyl)-1-(3,4-methylenedioxyphenyl)ethanol

Base Information

Chemical Name:2-(2-hydroxymethyl-3,4-dimethoxyphenyl)-1-(3,4-methylenedioxyphenyl)ethanol
CAS No.:114475-85-3
Molecular Formula:C₁₈H₂₀O₆
Molecular Weight:332.353
Hs Code.:

Synonyms:2-(2-hydroxymethyl-3,4-dimethoxyphenyl)-1-(3,4-methylenedioxyphenyl)ethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-hydroxymethyl-3,4-dimethoxyphenyl)-1-(3,4-methylenedioxyphenyl)ethanol

Chemical Property:

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Technology Process of 2-(2-hydroxymethyl-3,4-dimethoxyphenyl)-1-(3,4-methylenedioxyphenyl)ethanol

There total 5 articles about 2-(2-hydroxymethyl-3,4-dimethoxyphenyl)-1-(3,4-methylenedioxyphenyl)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 114475-89-7
3,4-dihydro-7,8-dimethoxy-3-(3,4-methylenedioxyphenyl)isocoumarin

: 114475-85-3
2-(2-hydroxymethyl-3,4-dimethoxyphenyl)-1-(3,4-methylenedioxyphenyl)ethanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 5h; Heating;

Reference yield:

: 106367-88-8
6-(chloromethyl)-2,3-dimethoxybenzoic acid methyl ester

: 114475-85-3
2-(2-hydroxymethyl-3,4-dimethoxyphenyl)-1-(3,4-methylenedioxyphenyl)ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / zinc chloride, naphthalene, lithium, 10percent hydrochloric acid / 1,2-dimethoxy-ethane / 1 h

2: 97 percent / lithium aluminum hydride / tetrahydrofuran / 5 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; naphthalene; lithium; zinc(II) chloride; In tetrahydrofuran; 1,2-dimethoxyethane;

Reference yield:

: 56579-86-3
2-(3,4-methylenedioxyphenyl)-1,3-dithiane

: 114475-85-3
2-(2-hydroxymethyl-3,4-dimethoxyphenyl)-1-(3,4-methylenedioxyphenyl)ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) butyllithium / 1.) THF, hexane, -78 deg C, 1 h; 2.) THF, -78 deg C to r.t., 3 h

2: 85 percent / glyoxylic acid hydrate, conc. hydrochloric acid / acetic acid / 1.) steam-bath, 20 min; 2.) r.t., 18 h

3: LiAlH₄

With hydrogenchloride; lithium aluminium tetrahydride; n-butyllithium; Glyoxilic acid; In acetic acid;