2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid benzyl ester

Base Information

Chemical Name:2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid benzyl ester
CAS No.:220758-99-6
Molecular Formula:C₄₁H₅₂N₄O₄
Molecular Weight:664.888
Hs Code.:

2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[<i>cd</i>]indene-6-carboxylic acid benzyl ester

Synonyms:2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid benzyl ester

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Chemical Property of 2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid benzyl ester

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Technology Process of 2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid benzyl ester

There total 3 articles about 2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 220758-98-5
2a,7b-bis-(4-heptyl-phenyl)-2,3-bis-(4-methoxy-benzyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid benzyl ester

: 220758-99-6
2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid benzyl ester

Guidance literature:: With ammonium cerium(IV) nitrate; In water; acetonitrile; for 24h; Ambient temperature;
DOI:10.1002/(SICI)1521-3773(19981231)37:24<3410::AID-ANIE3410>3.0.CO;2-1

Reference yield:

: 130543-50-9
2-bromomethylacrylic acid benzyl ester

: 220758-99-6
2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / Cs₂CO₃ / acetonitrile / 3 h / Heating

2: 62 percent / CAN / acetonitrile; H₂O / 24 h / Ambient temperature

With ammonium cerium(IV) nitrate; caesium carbonate; In water; acetonitrile;
DOI:10.1002/(SICI)1521-3773(19981231)37:24<3410::AID-ANIE3410>3.0.CO;2-1

Reference yield:

: 3a,6a-bis-(4-heptyl-phenyl)-1,6-bis-(4-methoxy-benzyl)-tetrahydro-imidazo[4,5-d]imidazole-2,5-dione

: 220758-99-6
2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / Cs₂CO₃ / acetonitrile / 3 h / Heating

2: 62 percent / CAN / acetonitrile; H₂O / 24 h / Ambient temperature

With ammonium cerium(IV) nitrate; caesium carbonate; In water; acetonitrile;
DOI:10.1002/(SICI)1521-3773(19981231)37:24<3410::AID-ANIE3410>3.0.CO;2-1