2-bromomethylacrylic acid benzyl ester

Base Information

Chemical Name:2-bromomethylacrylic acid benzyl ester
CAS No.:130543-50-9
Molecular Formula:C₁₁H₁₁BrO₂
Molecular Weight:255.111
Hs Code.:

Synonyms:2-bromomethylacrylic acid benzyl ester

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Chemical Property of 2-bromomethylacrylic acid benzyl ester

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Technology Process of 2-bromomethylacrylic acid benzyl ester

There total 4 articles about 2-bromomethylacrylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 385817-43-6
2-hydroxymethylacrylic acid benzyl ester

: 130543-50-9
2-bromomethylacrylic acid benzyl ester

Guidance literature:: With phosphorus tribromide; In diethyl ether; at 20 ℃; for 6h;
DOI:10.1021/ja011651d

Reference yield:

: 7396-44-3
benzyl diethylphosphonoacetate

: 130543-50-9
2-bromomethylacrylic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 32 percent / K₂CO₃ / H₂O / 2 h / 20 °C

2: 90 percent / PBr₃ / diethyl ether / 6 h / 20 °C

With phosphorus tribromide; potassium carbonate; In diethyl ether; water;
DOI:10.1021/ja011651d

Reference yield:

: 5437-45-6
Benzyl bromoacetate

: 130543-50-9
2-bromomethylacrylic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / 1 h / 200 °C

2: 32 percent / K₂CO₃ / H₂O / 2 h / 20 °C

3: 90 percent / PBr₃ / diethyl ether / 6 h / 20 °C

With phosphorus tribromide; potassium carbonate; In diethyl ether; water;
DOI:10.1021/ja011651d