methyl 2-(3-{tert-butyldiphenylsilyloxy}propyl)-1,3-oxazole-4-carboxylate

Base Information

Chemical Name:methyl 2-(3-{tert-butyldiphenylsilyloxy}propyl)-1,3-oxazole-4-carboxylate
CAS No.:233750-51-1
Molecular Formula:C₂₄H₂₉NO₄Si
Molecular Weight:423.584
Hs Code.:

Synonyms:methyl 2-(3-{tert-butyldiphenylsilyloxy}propyl)-1,3-oxazole-4-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-(3-{tert-butyldiphenylsilyloxy}propyl)-1,3-oxazole-4-carboxylate

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Technology Process of methyl 2-(3-{tert-butyldiphenylsilyloxy}propyl)-1,3-oxazole-4-carboxylate

There total 6 articles about methyl 2-(3-{tert-butyldiphenylsilyloxy}propyl)-1,3-oxazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1238759-83-5
methyl 2-(3-((tert-butyldiphenylsilyl)oxy)propyl)-2,5-dihydrooxazole-4-carboxylate

: 233750-51-1
methyl 2-(3-{tert-butyldiphenylsilyloxy}propyl)-1,3-oxazole-4-carboxylate

Guidance literature:: With N-Bromosuccinimide; potassium carbonate; In 1,2-dichloro-ethane; for 0.5h; Reflux; Inert atmosphere;
DOI:10.1021/ol1012789

Reference yield: 78.0%

: 853406-71-0
2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-4,5-dihydro-oxazole-4-carboxylic acid methyl ester

: 233750-51-1
methyl 2-(3-{tert-butyldiphenylsilyloxy}propyl)-1,3-oxazole-4-carboxylate

Guidance literature:: With Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1021/ol050543j

Reference yield: 54.0%

: 233750-49-7
methyl 3-hydroxy-2-[(4-{tert-butyldiphenylsilyloxy}butanoyl)amino]propanoate

: 233750-51-1
methyl 2-(3-{tert-butyldiphenylsilyloxy}propyl)-1,3-oxazole-4-carboxylate

Guidance literature:: methyl 3-hydroxy-2-[(4-{tert-butyldiphenylsilyloxy}butanoyl)amino]propanoate; With diethylamino-sulfur trifluoride; In dichloromethane; at -78 ℃; for 2h;

With potassium carbonate; In dichloromethane; at -20 ℃; for 1h;

With Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 - 20 ℃; for 10h; Inert atmosphere;
DOI:10.1016/j.bmc.2012.02.018