Technology Process of C33H39N3O6
There total 5 articles about C33H39N3O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C25H25NO7;
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
N,N-dimethyl acetamide;
at 0 ℃;
for 1h;
Inert atmosphere;
4-aminomethylquinuclidine;
In
N,N-dimethyl acetamide;
at 0 ℃;
for 1h;
Overall yield = 1.59 g;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium iodide; potassium carbonate / N,N-dimethyl acetamide / 1.5 h / 50 °C / Inert atmosphere
2.1: pyridine; selenium(IV) oxide / 24 h / 80 °C / Inert atmosphere
3.1: triethylamine / methanol / 5.5 h / 0 °C / Inert atmosphere
4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl acetamide / 1 h / 0 °C / Inert atmosphere
4.2: 1 h / 0 °C / Inert atmosphere
With
pyridine; selenium(IV) oxide; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium iodide;
In
methanol; N,N-dimethyl acetamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium iodide; potassium carbonate / N,N-dimethyl acetamide / 1.5 h / 50 °C / Inert atmosphere
2.1: pyridine; selenium(IV) oxide / 24 h / 80 °C / Inert atmosphere
3.1: triethylamine / methanol / 5.5 h / 0 °C / Inert atmosphere
4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl acetamide / 1 h / 0 °C / Inert atmosphere
4.2: 1 h / 0 °C / Inert atmosphere
With
pyridine; selenium(IV) oxide; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium iodide;
In
methanol; N,N-dimethyl acetamide;