8-(4-benzoylphenyloxy)-geraniol

Base Information

Chemical Name:8-(4-benzoylphenyloxy)-geraniol
CAS No.:196312-06-8
Molecular Formula:C₂₃H₂₆O₃
Molecular Weight:350.458
Hs Code.:

Synonyms:8-(4-benzoylphenyloxy)-geraniol

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Chemical Property of 8-(4-benzoylphenyloxy)-geraniol

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Technology Process of 8-(4-benzoylphenyloxy)-geraniol

There total 4 articles about 8-(4-benzoylphenyloxy)-geraniol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 196312-05-7
{4-[(2E,6E)-8-(tert-Butyl-dimethyl-silanyloxy)-2,6-dimethyl-octa-2,6-dienyloxy]-phenyl}-phenyl-methanone

: 196312-06-8
8-(4-benzoylphenyloxy)-geraniol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/ja036178d

Reference yield:

: 80873-81-0
geraniol tert-butyldimethylsilyl ether

: 196312-06-8
8-(4-benzoylphenyloxy)-geraniol

Guidance literature:: Multi-step reaction with 3 steps

1.1: SeO₂; t-BuOOH; salycylic acid / CH₂Cl₂; H₂O; various solvent(s) / 12 h

1.2: 50 percent / NaBH₄ / methanol

2.1: 81 percent / PPh₃; diethylazodicarboxylate / tetrahydrofuran / 20 °C

3.1: 97 percent / TBAF / tetrahydrofuran / 1 h / 0 °C

With tert.-butylhydroperoxide; selenium(IV) oxide; tetrabutyl ammonium fluoride; triphenylphosphine; salicylic acid; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ja036178d

Reference yield:

: 127586-84-9
8-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-2,6-dimethyl-2(E),6(E)-octadien-1-ol

: 196312-06-8
8-(4-benzoylphenyloxy)-geraniol

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / PPh₃; diethylazodicarboxylate / tetrahydrofuran / 20 °C

2: 97 percent / TBAF / tetrahydrofuran / 1 h / 0 °C

With tetrabutyl ammonium fluoride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1021/ja036178d