Technology Process of C25H31NO6S
There total 4 articles about C25H31NO6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: aluminum (III) chloride / Inert atmosphere
2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere; Cooling with ice
3.1: toluene-4-sulfonic acid / toluene / Inert atmosphere; Reflux
4.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C / Inert atmosphere
4.2: 20 °C / Inert atmosphere
4.3: Inert atmosphere
With
aluminum (III) chloride; sodium hydride; toluene-4-sulfonic acid; lithium diisopropyl amide;
In
tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tet.2011.10.022
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: toluene-4-sulfonic acid / toluene / Inert atmosphere; Reflux
2.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere
2.3: Inert atmosphere
With
toluene-4-sulfonic acid; lithium diisopropyl amide;
In
tetrahydrofuran; toluene;
DOI:10.1016/j.tet.2011.10.022
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere; Cooling with ice
2.1: toluene-4-sulfonic acid / toluene / Inert atmosphere; Reflux
3.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
3.3: Inert atmosphere
With
sodium hydride; toluene-4-sulfonic acid; lithium diisopropyl amide;
In
tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tet.2011.10.022