2-(3,5-bis(trifluoromethyl)phenyl)-N-(2-chlorophenyl)-N-methyl-2-oxoacetamide

Base Information

Chemical Name:2-(3,5-bis(trifluoromethyl)phenyl)-N-(2-chlorophenyl)-N-methyl-2-oxoacetamide
CAS No.:1309455-52-4
Molecular Formula:C₁₇H₁₀ClF₆NO₂
Molecular Weight:409.715
Hs Code.:

Synonyms:2-(3,5-bis(trifluoromethyl)phenyl)-N-(2-chlorophenyl)-N-methyl-2-oxoacetamide

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Chemical Property of 2-(3,5-bis(trifluoromethyl)phenyl)-N-(2-chlorophenyl)-N-methyl-2-oxoacetamide

Chemical Property:

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Technology Process of 2-(3,5-bis(trifluoromethyl)phenyl)-N-(2-chlorophenyl)-N-methyl-2-oxoacetamide

There total 4 articles about 2-(3,5-bis(trifluoromethyl)phenyl)-N-(2-chlorophenyl)-N-methyl-2-oxoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₈ClF₆NO₂

: 74-88-4
methyl iodide

: 1309455-52-4
2-(3,5-bis(trifluoromethyl)phenyl)-N-(2-chlorophenyl)-N-methyl-2-oxoacetamide

Guidance literature:: C₁₆H₈ClF₆NO₂; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃;

methyl iodide; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1002/chem.201100256

Reference yield:

: C₁₀H₃ClF₆O₂

: 1309455-52-4
2-(3,5-bis(trifluoromethyl)phenyl)-N-(2-chlorophenyl)-N-methyl-2-oxoacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran / 0 - 20 °C

2.2: 0 - 20 °C

With sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201100256

Reference yield:

: 374794-68-0
3,5-bis(trifluoromethyl)benzoylformic acid

: 1309455-52-4
2-(3,5-bis(trifluoromethyl)phenyl)-N-(2-chlorophenyl)-N-methyl-2-oxoacetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C

2.1: triethylamine / dichloromethane / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran / 0 - 20 °C

3.2: 0 - 20 °C

With oxalyl dichloride; sodium hydride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201100256