C₂₃H₁₈Cl₂O₄Si

Base Information

Chemical Name:C₂₃H₁₈Cl₂O₄Si
CAS No.:1393818-08-0
Molecular Formula:C₂₃H₁₈Cl₂O₄Si
Molecular Weight:457.385
Hs Code.:

C<sub>23</sub>H<sub>18</sub>Cl<sub>2</sub>O<sub>4</sub>Si

Synonyms:C₂₃H₁₈Cl₂O₄Si

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Chemical Property of C₂₃H₁₈Cl₂O₄Si

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Technology Process of C₂₃H₁₈Cl₂O₄Si

There total 10 articles about C₂₃H₁₈Cl₂O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 591-19-5
m-Bromoaniline

: 1393818-08-0
C₂₃H₁₈Cl₂O₄Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium carbonate / acetonitrile / 80 °C

2.1: acetic acid / 80 °C

3.1: sec.-butyllithium / tetrahydrofuran / -78 °C

3.2: -78 - 20 °C

3.3: 20 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,3-dimethylbarbituric acid / dichloromethane / 20 °C

5.1: water; sodium nitrite; sulfuric acid / methanol / 0 °C

5.2: Reflux

6.1: sodium hypochlorite; sodium hydroxide / water; methanol / 1 h / 20 °C

7.1: 1H-imidazole / dichloromethane / 20 °C

8.1: sec.-butyllithium / tetrahydrofuran / 0.33 h / -78 °C / Inert atmosphere

8.2: 0.5 h / -78 - 20 °C / Inert atmosphere

9.1: hydrogenchloride; water / methanol / 0.33 h / 20 °C

10.1: trifluoroacetic acid / 2 h

With 1H-imidazole; hydrogenchloride; sodium hypochlorite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,3-dimethylbarbituric acid; sulfuric acid; water; sec.-butyllithium; potassium carbonate; trifluoroacetic acid; sodium hydroxide; sodium nitrite; In tetrahydrofuran; methanol; dichloromethane; water; acetic acid; acetonitrile;
DOI:10.1002/anie.201210279

Reference yield:

$5,13-dihydroxy-2,2-dimethyl-2-silatricyclo[8.4.0.0^{3,8}]tetradeca-1<sup>(10)</sup>,3,5,7,11,13-hexaen-9-one$: 1301205-24-2
5,13-dihydroxy-2,2-dimethyl-2-silatricyclo[8.4.0.0^{3,8}]tetradeca-1⁽¹⁰⁾,3,5,7,11,13-hexaen-9-one

: 1393818-08-0
C₂₃H₁₈Cl₂O₄Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hypochlorite; sodium hydroxide / water; methanol / 1 h / 20 °C

2.1: 1H-imidazole / dichloromethane / 20 °C

3.1: sec.-butyllithium / tetrahydrofuran / 0.33 h / -78 °C / Inert atmosphere

3.2: 0.5 h / -78 - 20 °C / Inert atmosphere

4.1: hydrogenchloride; water / methanol / 0.33 h / 20 °C

5.1: trifluoroacetic acid / 2 h

With 1H-imidazole; hydrogenchloride; sodium hypochlorite; water; sec.-butyllithium; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/anie.201210279

Reference yield:

: 1391714-51-4
4,5-dichloro-10,10-dimethyl-10-sila-3,6-bis((tert-butyldimethylsilyl)oxy)-9H-xanthen-9-one

: 1393818-08-0
C₂₃H₁₈Cl₂O₄Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: sec.-butyllithium / tetrahydrofuran / 0.33 h / -78 °C / Inert atmosphere

1.2: 0.5 h / -78 - 20 °C / Inert atmosphere

2.1: hydrogenchloride; water / methanol / 0.33 h / 20 °C

3.1: trifluoroacetic acid / 2 h

With hydrogenchloride; water; sec.-butyllithium; trifluoroacetic acid; In tetrahydrofuran; methanol;
DOI:10.1002/anie.201210279