(p-sulfophenyl) glyoxylic acid

Base Information

• Chemical Name: (p-sulfophenyl) glyoxylic acid
• CAS No.: 134653-58-0
• Molecular Formula: C₈H₆O₆S
• Molecular Weight: 230.198

Synonyms:(p-sulfophenyl) glyoxylic acid

Chemical Property of (p-sulfophenyl) glyoxylic acid

Chemical Property:

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Technology Process of (p-sulfophenyl) glyoxylic acid

There total 3 articles about (p-sulfophenyl) glyoxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(p-sulfophenyl)glycine (124755-49-3) → ammonia (7664-41-7) + (p-sulfophenyl) glyoxylic acid (134653-58-0)

Guidance literature:

With pyridoxal 5'-phosphate; copper(II) ion; oxygen; Cu{SO₃C₆H₄CH(COO)NCH(C₅HN)O(CH₃)2(OH)}^(2-); In water; oxidative deamination in basic aq. soln. in presence of 0.10 M Cu(2+) and 3, 5'-deoxypyridoxal; molecular O2 is bubbled through; evolution of ammonia; catalyst is prepared in situ; reaction is complete after 15 d;; ammonia was detected by Nessler's test; keto acid is recrystd. from hot water and charcaterized by (1)H- and (13)C-NMR;;

DOI:10.1021/ja00017a019

Reference yield:

Cu{SO3C6H4CH(COO)NCH(C5HN)O(CH3)2(OH)}(2-) → Cu(2+)*HONCH(C5HN)O(CH3)2(1-)=Cu{HONCH(C5HN)O(CH3)2}(1+) + (p-sulfophenyl) glyoxylic acid (134653-58-0)

Guidance literature:

With oxygen; In water; uptake of O2 above pH 9; Cu-Schiff base complex disappears; oxime complex is formed;; detected by UV/Vis spectroscopy;; Kinetics;

DOI:10.1021/ja00017a019

Reference yield:

(p-sulfophenyl)glycine (124755-49-3) → (p-sulfophenyl) glyoxylic acid (134653-58-0)

Guidance literature:

With pyridoxal 5'-phosphate; oxygen; copper(II) nitrate; In water; at 25 ℃; Rate constant; Mechanism; other reagents, var. temperature, pH;

DOI:10.1021/ja00017a019

upstream raw materials:

(p-sulfophenyl)glycine

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