(S)-6-((6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)methyl)-2,3-dimethoxylbenzyl acetate

Base Information

Chemical Name:(S)-6-((6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)methyl)-2,3-dimethoxylbenzyl acetate
CAS No.:1422431-15-9
Molecular Formula:C₂₃H₂₉NO₆
Molecular Weight:415.486
Hs Code.:

Synonyms:(S)-6-((6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)methyl)-2,3-dimethoxylbenzyl acetate

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Chemical Property of (S)-6-((6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)methyl)-2,3-dimethoxylbenzyl acetate

Chemical Property:

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Technology Process of (S)-6-((6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)methyl)-2,3-dimethoxylbenzyl acetate

There total 3 articles about (S)-6-((6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)methyl)-2,3-dimethoxylbenzyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6-((6,7-dimethoxy-3,4-dihydroisoquinolin-1-yl)methyl)-2,3-dimethoxyphenyl acetate

: 1422431-15-9
(S)-6-((6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)methyl)-2,3-dimethoxylbenzyl acetate

Guidance literature:: With (1S,2S)-(+)-N-tosyl-1,2-diphenylethane-1,2-diamine[η6-1-isopropyl-4-methylbenzene]-ruthenium(II); formic acid; triethylamine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.bmc.2012.12.016

Reference yield:

: C₂₃H₂₇NO₆

: 1422431-15-9
(S)-6-((6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)methyl)-2,3-dimethoxylbenzyl acetate

Guidance literature:: With formic acid; triethylamine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.bmcl.2017.01.090

Reference yield:

: 1422431-12-6
6-(2-(3,4-dimethoxyphenethylamino)-2-oxoethyl)-2,3-dimethoxyphenyl acetate

: 1422431-15-9
(S)-6-((6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)methyl)-2,3-dimethoxylbenzyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / acetonitrile / Reflux

2: triethylamine; formic acid / N,N-dimethyl-formamide / 20 °C

With formic acid; triethylamine; trichlorophosphate; In N,N-dimethyl-formamide; acetonitrile; 1: |Bischler-Napieralski Reaction;
DOI:10.1016/j.bmcl.2017.01.090