2-(4-acetylamino-phenylsulfanyl)-5-nitro-benzenesulfonic acid amide

Base Information

• Chemical Name: 2-(4-acetylamino-phenylsulfanyl)-5-nitro-benzenesulfonic acid amide
• CAS No.: 861062-46-6
• Molecular Formula: C₁₄H₁₃N₃O₅S₂
• Molecular Weight: 367.406
• Mol file: 861062-46-6.mol

Synonyms:2-(4-acetylamino-phenylsulfanyl)-5-nitro-benzenesulfonic acid amide

Chemical Property of 2-(4-acetylamino-phenylsulfanyl)-5-nitro-benzenesulfonic acid amide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 2-(4-acetylamino-phenylsulfanyl)-5-nitro-benzenesulfonic acid amide

There total 3 articles about 2-(4-acetylamino-phenylsulfanyl)-5-nitro-benzenesulfonic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

S-[4-(acetylamino)phenyl] ethanethioate (946-94-1) → 2-(4-acetylamino-phenylsulfanyl)-5-nitro-benzenesulfonic acid amide (861062-46-6)

Guidance literature:

Multi-step reaction with 2 steps

1: aq.-ethanolic NaOH

With sodium hydroxide;

DOI:10.1021/jo01148a027

Reference yield:

4-chlorobenzonitrile (100-00-5) → 2-(4-acetylamino-phenylsulfanyl)-5-nitro-benzenesulfonic acid amide (861062-46-6)

Guidance literature:

Multi-step reaction with 3 steps

1: aqueous Na₂S / und anschliessend mit Acetanhydrid

2: aq.-ethanolic NaOH

With sodium sulfide; sodium hydroxide;

DOI:10.1021/jo01148a027

Reference yield:

2-chloro-5-nitrobenzenesulfonamide (96-72-0) + 4-acetamidothiophenol (1126-81-4) → 2-(4-acetylamino-phenylsulfanyl)-5-nitro-benzenesulfonic acid amide (861062-46-6)

Guidance literature:

DOI:10.1021/jo01148a027

upstream raw materials:

2-chloro-5-nitrobenzenesulfonamide

4-acetamidothiophenol

S-[4-(acetylamino)phenyl] ethanethioate

4-chlorobenzonitrile

Downstream raw materials:

2-(N-acetyl-sulfanilyl)-5-amino-benzenesulfonic acid amide

5-amino-2-sulfanilyl-benzenesulfonic acid amide

2-(N-acetyl-sulfanilyl)-5-nitro-benzenesulfonic acid amide