N-{4-[4-amino-6,7-dimethyl-2-({[(1-methylethylidene)amino]oxy}methyl)-1H-imidazo[4,5-c]pyridin-1-yl]butyl}-N-cyclohexylurea hydrochloride

Base Information

Chemical Name:N-{4-[4-amino-6,7-dimethyl-2-({[(1-methylethylidene)amino]oxy}methyl)-1H-imidazo[4,5-c]pyridin-1-yl]butyl}-N-cyclohexylurea hydrochloride
CAS No.:852801-96-8
Molecular Formula:C₂₃H₃₇N₇O₂*ClH
Molecular Weight:480.053
Hs Code.:

Synonyms:N-{4-[4-amino-6,7-dimethyl-2-({[(1-methylethylidene)amino]oxy}methyl)-1H-imidazo[4,5-c]pyridin-1-yl]butyl}-N-cyclohexylurea hydrochloride

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Chemical Property of N-{4-[4-amino-6,7-dimethyl-2-({[(1-methylethylidene)amino]oxy}methyl)-1H-imidazo[4,5-c]pyridin-1-yl]butyl}-N-cyclohexylurea hydrochloride

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Technology Process of N-{4-[4-amino-6,7-dimethyl-2-({[(1-methylethylidene)amino]oxy}methyl)-1H-imidazo[4,5-c]pyridin-1-yl]butyl}-N-cyclohexylurea hydrochloride

There total 7 articles about N-{4-[4-amino-6,7-dimethyl-2-({[(1-methylethylidene)amino]oxy}methyl)-1H-imidazo[4,5-c]pyridin-1-yl]butyl}-N-cyclohexylurea hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 852800-04-5
N-{4-[4-amino-6,7-dimethyl-2-({[(1-methylethylidene)amino]oxy}methyl)-1H-imidazo[4,5-c]pyridin-1-yl]butyl}-N-cyclohexylurea

: 852801-96-8
N-{4-[4-amino-6,7-dimethyl-2-({[(1-methylethylidene)amino]oxy}methyl)-1H-imidazo[4,5-c]pyridin-1-yl]butyl}-N-cyclohexylurea hydrochloride

Guidance literature:: With hydrogenchloride; In water;

Reference yield:

: 437384-55-9
2,4-Dichloro-5,6-Dimethyl-3-nitro-pyridine

: 852801-96-8
N-{4-[4-amino-6,7-dimethyl-2-({[(1-methylethylidene)amino]oxy}methyl)-1H-imidazo[4,5-c]pyridin-1-yl]butyl}-N-cyclohexylurea hydrochloride

Guidance literature:: Multi-step reaction with 11 steps

1.1: triethylamine / N,N-dimethyl-formamide / 20 °C

2.1: sodium azide; cerium(III) chloride / water; acetonitrile / 72 h / Heating / reflux

3.1: hydrogen / palladium 10% on activated carbon / acetonitrile / 5 h

4.1: chloroform / 72 h

5.1: hydrogenchloride; water / methanol / 2 h / 20 °C

6.1: triethylamine / dichloromethane / 20 °C

7.1: triethylamine / N,N-dimethyl-formamide

8.1: hydrazine / ethanol; dichloromethane / 2 h

8.2: 2 h / 20 °C

9.1: 1,2-dichloro-benzene / 72 h / 20 - 120 °C

10.1: water; acetic acid / methanol / 504 h / 50 - 55 °C

11.1: hydrogenchloride / water

With hydrogenchloride; sodium azide; cerium(III) chloride; water; hydrogen; acetic acid; triethylamine; hydrazine; palladium 10% on activated carbon; In methanol; ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; 1,2-dichloro-benzene; acetonitrile;

Reference yield:

: 852719-28-9
tert-butyl 4-[(5,6-dimethyl-8-nitrotetraazolo[1,5-a]pyridin-7-yl)amino]butylcarbamate

: 852801-96-8
N-{4-[4-amino-6,7-dimethyl-2-({[(1-methylethylidene)amino]oxy}methyl)-1H-imidazo[4,5-c]pyridin-1-yl]butyl}-N-cyclohexylurea hydrochloride

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrogen / palladium 10% on activated carbon / acetonitrile / 5 h

2.1: chloroform / 72 h

3.1: hydrogenchloride; water / methanol / 2 h / 20 °C

4.1: triethylamine / dichloromethane / 20 °C

5.1: triethylamine / N,N-dimethyl-formamide

6.1: hydrazine / ethanol; dichloromethane / 2 h

6.2: 2 h / 20 °C

7.1: 1,2-dichloro-benzene / 72 h / 20 - 120 °C

8.1: water; acetic acid / methanol / 504 h / 50 - 55 °C

9.1: hydrogenchloride / water

With hydrogenchloride; water; hydrogen; acetic acid; triethylamine; hydrazine; palladium 10% on activated carbon; In methanol; ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; 1,2-dichloro-benzene; acetonitrile;