1,6:2,3-dianhydro-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-β-D-mannopyranose

Base Information

Chemical Name:1,6:2,3-dianhydro-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-β-D-mannopyranose
CAS No.:127529-87-7
Molecular Formula:C₃₅H₃₈O₁₀
Molecular Weight:618.681
Hs Code.:

Synonyms:1,6:2,3-dianhydro-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-β-D-mannopyranose

Suppliers and Price of 1,6:2,3-dianhydro-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-β-D-mannopyranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,6:2,3-dianhydro-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-β-D-mannopyranose

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,6:2,3-dianhydro-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-β-D-mannopyranose

There total 1 articles about 1,6:2,3-dianhydro-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-β-D-mannopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

: 3868-03-9
1,6:2,3-dianhydro-β-D-mannopyranose

: 61236-82-6
6-O-acetyl-2,3,4-tri-O-benzyl-α-D-galactopyranosyl bromide

: 127529-87-7
1,6:2,3-dianhydro-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-β-D-mannopyranose

: 1,6:2,3-dianhydro-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-galactopyranosyl)-β-D-mannopyranose

Guidance literature:: 4 A molecular sieve; silver silicate aluminate; In dichloromethane; toluene; at -55 ℃; for 2h;

Reference yield: 89.0%

: 127529-87-7
1,6:2,3-dianhydro-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-β-D-mannopyranose

: 127529-76-4
1,6-anhydro-2-azido-2-deoxy-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranose

Guidance literature:: With lithium azide; lutidine; triisopropylbenzenesulfonic acid; In N,N-dimethyl-formamide; at 100 ℃; for 24h;

Reference yield:

: 127529-87-7
1,6:2,3-dianhydro-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-β-D-mannopyranose

: 1,6-anhydro-2-azido-2-deoxy-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / LiN₃, triisopropylbenzenesulfonic acid, lutidine / dimethylformamide / 24 h / 100 °C

2: 40 percent / trimethylsilyl triflate, molecular sieves 4 Angstroem / diethyl ether; CH₂Cl₂ / 0.17 h / -30 °C

With lithium azide; lutidine; triisopropylbenzenesulfonic acid; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;