4-(3-Bromopropyl)-1-<(tert-butyldimethylsilyl)oxy>-2,6-dimethoxybenzene

Base Information

Chemical Name:4-(3-Bromopropyl)-1-<(tert-butyldimethylsilyl)oxy>-2,6-dimethoxybenzene
CAS No.:118631-00-8
Molecular Formula:C₁₇H₂₉BrO₃Si
Molecular Weight:389.405
Hs Code.:

Synonyms:4-(3-Bromopropyl)-1-<(tert-butyldimethylsilyl)oxy>-2,6-dimethoxybenzene

Suppliers and Price of 4-(3-Bromopropyl)-1-<(tert-butyldimethylsilyl)oxy>-2,6-dimethoxybenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(3-Bromopropyl)-1-<(tert-butyldimethylsilyl)oxy>-2,6-dimethoxybenzene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(3-Bromopropyl)-1-<(tert-butyldimethylsilyl)oxy>-2,6-dimethoxybenzene

There total 4 articles about 4-(3-Bromopropyl)-1-<(tert-butyldimethylsilyl)oxy>-2,6-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 158555-84-1
3-<4-<(tert-Butyldimethylsilyl)oxy>-3,5-dimethoxyphenyl>-1-propanol

: 118631-00-8
4-(3-Bromopropyl)-1-<(tert-butyldimethylsilyl)oxy>-2,6-dimethoxybenzene

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In diethyl ether; for 4h; Yield given; Ambient temperature;
DOI:10.1021/jo00100a039

Reference yield:

: 6627-88-9
4-allyl-2,6-dimethoxyphenol

: 118631-00-8
4-(3-Bromopropyl)-1-<(tert-butyldimethylsilyl)oxy>-2,6-dimethoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / dimethylformamide / 4 h / Ambient temperature

2: 1.) BH₃*THF, 2.) 30percent H₂O₂, 3 N NaOH / 1.) THF, 0 deg C, 10 min; 2 h, 2.) 0 deg C, 15 min; 1 h

3: Ph₃P, CBr₄ / diethyl ether / 4 h / Ambient temperature

With 1H-imidazole; sodium hydroxide; borane-THF; carbon tetrabromide; dihydrogen peroxide; triphenylphosphine; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/jo00100a039

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 118631-00-8
4-(3-Bromopropyl)-1-<(tert-butyldimethylsilyl)oxy>-2,6-dimethoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / dimethylformamide / 4 h / Ambient temperature

2: 1.) BH₃*THF, 2.) 30percent H₂O₂, 3 N NaOH / 1.) THF, 0 deg C, 10 min; 2 h, 2.) 0 deg C, 15 min; 1 h

3: Ph₃P, CBr₄ / diethyl ether / 4 h / Ambient temperature

With 1H-imidazole; sodium hydroxide; borane-THF; carbon tetrabromide; dihydrogen peroxide; triphenylphosphine; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/jo00100a039