(1-(2-pyrimidyl)-3-(2,6-diisopropylphenyl))imidazolium chloride

Base Information

• Chemical Name: (1-(2-pyrimidyl)-3-(2,6-diisopropylphenyl))imidazolium chloride
• CAS No.: 1135618-74-4
• Molecular Formula: C₁₉H₂₃N₄*Cl
• Molecular Weight: 342.871
• Mol file: 1135618-74-4.mol

Synonyms:(1-(2-pyrimidyl)-3-(2,6-diisopropylphenyl))imidazolium chloride

Chemical Property of (1-(2-pyrimidyl)-3-(2,6-diisopropylphenyl))imidazolium chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1-(2-pyrimidyl)-3-(2,6-diisopropylphenyl))imidazolium chloride

There total 2 articles about (1-(2-pyrimidyl)-3-(2,6-diisopropylphenyl))imidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

2-chloropyrimidine (1722-12-9,1195939-87-7) + 1-(2,6-diisopropylphenyl)-1H-imidazole (25364-47-0) → (1-(2-pyrimidyl)-3-(2,6-diisopropylphenyl))imidazolium chloride (1135618-74-4)

Guidance literature:

at 120 ℃;

DOI:10.1021/om100670u

Reference yield:

2,6-diisopropylbenzenamine (24544-04-5) → (1-(2-pyrimidyl)-3-(2,6-diisopropylphenyl))imidazolium chloride (1135618-74-4)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphoric acid; ammonium chloride / methanol / Reflux

2: 120 °C

With phosphoric acid; ammonium chloride; In methanol;

DOI:10.1021/om100670u

Reference yield: 88.0%

(1-(2-pyrimidyl)-3-(2,6-diisopropylphenyl))imidazolium chloride (1135618-74-4) + silver(l) oxide (20667-12-3) → bis[(1-(2-pyrimidyl)-3-(2,6-diisopropylphenyl))imidazol-2-ylidene]silver(I) dichloroargenate

Guidance literature:

In dichloromethane; (N2) suspn. Ag2O and imidazolium salt in CH2Cl2 was stirred at room temp. overnight; soln. was filtered through Celite and concd. in vacuo;

DOI:10.1021/om100670u

upstream raw materials:

2-chloropyrimidine

1-(2,6-diisopropylphenyl)-1H-imidazole

2,6-diisopropylbenzenamine