p-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-tertbutyldiphenylsilyl-α-D-galactopyranoside

Base Information

Chemical Name:p-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-tertbutyldiphenylsilyl-α-D-galactopyranoside
CAS No.:1344980-45-5
Molecular Formula:C₅₀H₅₄O₇Si
Molecular Weight:795.06
Hs Code.:

Synonyms:p-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-tertbutyldiphenylsilyl-α-D-galactopyranoside

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Chemical Property of p-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-tertbutyldiphenylsilyl-α-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of p-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-tertbutyldiphenylsilyl-α-D-galactopyranoside

There total 3 articles about p-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-tertbutyldiphenylsilyl-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₃₆O₆SSi

: 100-39-0
benzyl bromide

: 1344980-45-5
p-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-tertbutyldiphenylsilyl-α-D-galactopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.carres.2012.02.021

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1344980-45-5
p-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-tertbutyldiphenylsilyl-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide / 6 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2012.02.021

Reference yield:

: 121468-39-1,12167-34-9
p-methoxyphenyl α-D-galactopyranoside

: 1344980-45-5
p-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-tertbutyldiphenylsilyl-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide / 6 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2012.02.021