tert-butyl-1-(cyclohexylmethyl)-2-(propan-2-ylidene)hydrazine carboxylate

Base Information

Chemical Name:tert-butyl-1-(cyclohexylmethyl)-2-(propan-2-ylidene)hydrazine carboxylate
CAS No.:1608125-58-1
Molecular Formula:C₁₅H₂₈N₂O₂
Molecular Weight:268.4
Hs Code.:

Synonyms:tert-butyl-1-(cyclohexylmethyl)-2-(propan-2-ylidene)hydrazine carboxylate

Suppliers and Price of tert-butyl-1-(cyclohexylmethyl)-2-(propan-2-ylidene)hydrazine carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tert-butyl-1-(cyclohexylmethyl)-2-(propan-2-ylidene)hydrazine carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl-1-(cyclohexylmethyl)-2-(propan-2-ylidene)hydrazine carboxylate

There total 2 articles about tert-butyl-1-(cyclohexylmethyl)-2-(propan-2-ylidene)hydrazine carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 16689-34-2
tert-butyl isopropylidenecarbazate

: 2550-36-9
Cyclohexylmethyl bromide

: 1608125-58-1
tert-butyl-1-(cyclohexylmethyl)-2-(propan-2-ylidene)hydrazine carboxylate

Guidance literature:: tert-butyl isopropylidenecarbazate; With tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide; In toluene; at 50 ℃; for 2h;

Cyclohexylmethyl bromide; In toluene; at 80 ℃; for 2h;
DOI:10.1016/j.bmc.2014.03.016

Reference yield:

: 870-46-2
t-butoxycarbonylhydrazine

: 1608125-58-1
tert-butyl-1-(cyclohexylmethyl)-2-(propan-2-ylidene)hydrazine carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium sulfate; acetic acid / 1 h / Reflux

2.1: potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / toluene / 2 h / 50 °C

2.2: 2 h / 80 °C

With tetra(n-butyl)ammonium hydrogensulfate; magnesium sulfate; acetic acid; potassium hydroxide; In toluene;
DOI:10.1016/j.bmc.2014.03.016