1-dodecenyl phenyl sulfide

Base Information

• Chemical Name: 1-dodecenyl phenyl sulfide
• CAS No.: 75712-22-0
• Molecular Formula: C₁₈H₂₈S
• Molecular Weight: 276.486

Synonyms:1-dodecenyl phenyl sulfide

Chemical Property of 1-dodecenyl phenyl sulfide

Chemical Property:

Purity/Quality:

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Technology Process of 1-dodecenyl phenyl sulfide

There total 7 articles about 1-dodecenyl phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

C24H34OS2 → 1-dodecenyl phenyl sulfide (75712-22-0)

Guidance literature:

In 1,2-dimethoxyethane; for 3h; Heating;

Reference yield: 81.0%

1-dodecyne (765-03-7) + thiophenol (108-98-5) → 1-dodecenyl phenyl sulfide (75712-22-0)

Guidance literature:

With triethyl borane; In hexane; benzene; at 25 ℃; for 4h;

DOI:10.1246/cl.1987.1647

Reference yield: 59.0%

triethyl borane (97-94-9) + thiophenol (108-98-5) + (E)-1-(triphenylstannyl)-1-dodecene (104849-58-3,104849-71-0) → 1-dodecenyl phenyl sulfide (75712-22-0)

Guidance literature:

In not given; treatment of stannane with PhSH/Et3B, reaction time 11h; ratio E/Z = 1/1;

DOI:10.1246/cl.1988.669

upstream raw materials:

1-dodecyne

thiophenol

C₂₄H₃₄S₂

triethyl borane

Downstream raw materials:

2-triphenylgermyl-1-dodecyl phenyl sulfide

(E)-1-triphenylgermyl-1-dodecene

1-triphenylstannyl-1-dodecene

1-phenylsulfinyl-1-dodecene

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