Germane, 1-dodecenyltriphenyl-, (E)-

Base Information

Chemical Name:Germane, 1-dodecenyltriphenyl-, (E)-
CAS No.:92740-99-3
Molecular Formula:C30H38Ge
Molecular Weight:471.222
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Germane, 1-dodecenyltriphenyl-, (E)-

Chemical Property:

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Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Germane, 1-dodecenyltriphenyl-, (E)-

There total 12 articles about Germane, 1-dodecenyltriphenyl-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: lithium tris(triphenylgermyl)manganate(II)

: 765-03-7
1-dodecyne

: 92740-99-3
(E)-1-triphenylgermyl-1-dodecene

Guidance literature:: With butan-1-ol; In tetrahydrofuran; 1-dodecyne (0.5 mmol) treated with germylmanganate (0.6 mmol) in THF inthe presence of n-BuOH (2.0 mmol) at 25°C for 4.5 h;
DOI:10.1246/bcsj.73.2159

Reference yield: 99.0%

: 765-03-7
1-dodecyne

: 2816-43-5
triphenylgermane

: 92740-99-3
(E)-1-triphenylgermyl-1-dodecene

Guidance literature:: triethyl borane; In hexane; benzene; addn. of Et3B in hexane to a soln. of acetylene-compd. and a slight excess of Ph3GeH in benzene, heating at 60°C for 2 h; evapn., purifn. by column chromy. or preparative thin-layer chromy. on silica gel,; elem. anal.; isomer ratio Z/E=<1/20 (detd. by GC, NMR);
DOI:10.1246/bcsj.63.2268