2-[(1S,3S)-3-(tert-butyldimethylsilyloxy)-2,2-dimethyl-6-methylidenecyclohexyl]iodoethane

Base Information

• Chemical Name: 2-[(1S,3S)-3-(tert-butyldimethylsilyloxy)-2,2-dimethyl-6-methylidenecyclohexyl]iodoethane
• CAS No.: 615562-18-0
• Molecular Formula: C₁₇H₃₃IOSi
• Molecular Weight: 408.438

Synonyms:2-[(1S,3S)-3-(tert-butyldimethylsilyloxy)-2,2-dimethyl-6-methylidenecyclohexyl]iodoethane

Chemical Property of 2-[(1S,3S)-3-(tert-butyldimethylsilyloxy)-2,2-dimethyl-6-methylidenecyclohexyl]iodoethane

Chemical Property:

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Technology Process of 2-[(1S,3S)-3-(tert-butyldimethylsilyloxy)-2,2-dimethyl-6-methylidenecyclohexyl]iodoethane

There total 3 articles about 2-[(1S,3S)-3-(tert-butyldimethylsilyloxy)-2,2-dimethyl-6-methylidenecyclohexyl]iodoethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1S,3S)-3-(tert-butyldimethylsilyloxy)-2,2-dimethyl-6-methylenecyclohexaneethanol (124263-03-2) → 2-[(1S,3S)-3-(tert-butyldimethylsilyloxy)-2,2-dimethyl-6-methylidenecyclohexyl]iodoethane (615562-18-0)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 4 °C

2: 5.91 g / NaI / acetone / 4 h / Heating

With pyridine; sodium iodide; In acetone;

DOI:10.1016/j.tet.2005.06.115

Reference yield:

tert-Butyl-{(1S,3S)-2,2-dimethyl-4-methylene-3-[2-(toluene-4-sulfonyl)-ethyl]-cyclohexyloxy}-dimethyl-silane → 2-[(1S,3S)-3-(tert-butyldimethylsilyloxy)-2,2-dimethyl-6-methylidenecyclohexyl]iodoethane (615562-18-0)

Guidance literature:

With sodium iodide; In acetone; Heating;

DOI:10.1016/S0040-4039(03)01669-1

Reference yield:

Toluene-4-sulfonic acid 2-[(1S,3S)-3-(tert-butyl-dimethyl-silanyloxy)-2,2-dimethyl-6-methylene-cyclohexyl]-ethyl ester → 2-[(1S,3S)-3-(tert-butyldimethylsilyloxy)-2,2-dimethyl-6-methylidenecyclohexyl]iodoethane (615562-18-0)

Guidance literature:

With sodium iodide; In acetone; for 4h; Heating;

DOI:10.1016/j.tet.2005.06.115

upstream raw materials:

(1S,3S)-3-(tert-butyldimethylsilyloxy)-2,2-dimethyl-6-methylenecyclohexaneethanol

Downstream raw materials:

6-{2-[(1S,3S)-3-(tert-butyldimethylsilyloxy)-2,2-dimethyl-6-methylidenecyclohexyl]ethyl}-1,4-dimethoxynaphthalene

(S)-3-[2-(5,8-Dimethoxy-naphthalen-2-yl)-ethyl]-2,2-dimethyl-4-methylene-cyclohexanone

(1S,3S)-3-[2-(5,8-Dimethoxy-naphthalen-2-yl)-ethyl]-2,2-dimethyl-4-methylene-cyclohexanol

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