thymidine cyclic 3'-5'-phosphoranilidate

Base Information

Chemical Name:thymidine cyclic 3'-5'-phosphoranilidate
CAS No.:76746-50-4
Molecular Formula:C₁₆H₁₈N₃O₆P
Molecular Weight:379.309
Hs Code.:

Synonyms:thymidine cyclic 3'-5'-phosphoranilidate

Suppliers and Price of thymidine cyclic 3'-5'-phosphoranilidate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of thymidine cyclic 3'-5'-phosphoranilidate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of thymidine cyclic 3'-5'-phosphoranilidate

There total 11 articles about thymidine cyclic 3'-5'-phosphoranilidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 65114-76-3
thymidine 3'-(2-chlorophenyl) phosphoranilidate

: 76746-50-4
thymidine cyclic 3'-5'-phosphoranilidate

Guidance literature:: With potassium tert-butylate; In N,N-dimethyl acetamide; for 20h; Ambient temperature;
DOI:10.1016/0040-4020(84)85099-1

Reference yield:

: 75444-14-3
3'-(4-Nitrophenyl N-phenyl phosphoramidate)-5'-monomethoxytrityl thimidine

: 76746-50-4
thymidine cyclic 3'-5'-phosphoranilidate

Guidance literature:: With acetic acid monohydrate; potassium tert-butylate; Multistep reaction; 2.) DMF, 45 min., room temp.;
DOI:10.1016/S0040-4039(00)93156-3

Reference yield:

: 42926-80-7
5'-O-(4-monomethoxytrityl)-2'-deoxythymidine

: 76746-50-4
thymidine cyclic 3'-5'-phosphoranilidate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 18 h / Ambient temperature

2: 80 percent / 2 percent toluene-p-sulphonic acid monohydrate / CHCl₃; methanol / 0.17 h / Ambient temperature

3: 90 percent / t-BuOK / N,N-dimethyl-acetamide / 20 h / Ambient temperature

With potassium tert-butylate; toluene-4-sulfonic acid; In pyridine; methanol; chloroform; N,N-dimethyl acetamide;
DOI:10.1016/0040-4020(84)85099-1