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Technology Process of 2,4,6-Me3C6H2NC3H2NCH2CH2NH-2,4,6-Me3C6H2

2,4,6-Me3C6H2NC3H2NCH2CH2NH-2,4,6-Me3C6H2

Base Information
  • Chemical Name:2,4,6-Me3C6H2NC3H2NCH2CH2NH-2,4,6-Me3C6H2
  • CAS No.:1057737-33-3
  • Molecular Formula:C23H29N3
  • Molecular Weight:347.503
  • Hs Code.:
2,4,6-Me<sub>3</sub>C<sub>6</sub>H<sub>2</sub>NC<sub>3</sub>H<sub>2</sub>NCH<sub>2</sub>CH<sub>2</sub>NH-2,4,6-Me<sub>3</sub>C<sub>6</sub>H<sub>2</sub>

Synonyms:2,4,6-Me3C6H2NC3H2NCH2CH2NH-2,4,6-Me3C6H2

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Chemical Property of 2,4,6-Me3C6H2NC3H2NCH2CH2NH-2,4,6-Me3C6H2
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Technology Process of 2,4,6-Me3C6H2NC3H2NCH2CH2NH-2,4,6-Me3C6H2

There total 1 articles about 2,4,6-Me3C6H2NC3H2NCH2CH2NH-2,4,6-Me3C6H2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1-(2,4,6-trimethylphenyl)-3-(2-((2,4,6-trimethylphenyl)amino)ethyl)imidazolium chloride
1057737-32-2

1-(2,4,6-trimethylphenyl)-3-(2-((2,4,6-trimethylphenyl)amino)ethyl)imidazolium chloride

2,4,6-Me<sub>3</sub>C<sub>6</sub>H<sub>2</sub>NC<sub>3</sub>H<sub>2</sub>NCH<sub>2</sub>CH<sub>2</sub>NH-2,4,6-Me<sub>3</sub>C<sub>6</sub>H<sub>2</sub>
1057737-33-3

2,4,6-Me3C6H2NC3H2NCH2CH2NH-2,4,6-Me3C6H2

Guidance literature:
With potassium hexamethylsilazane; In tetrahydrofuran; at 20 ℃;
DOI:10.1139/V08-082

Reference yield: 86.0%

Grubbs catalyst first generation

Grubbs catalyst first generation

2,4,6-Me<sub>3</sub>C<sub>6</sub>H<sub>2</sub>NC<sub>3</sub>H<sub>2</sub>NCH<sub>2</sub>CH<sub>2</sub>NH-2,4,6-Me<sub>3</sub>C<sub>6</sub>H<sub>2</sub>
1057737-33-3

2,4,6-Me3C6H2NC3H2NCH2CH2NH-2,4,6-Me3C6H2

[(2,4,6-Me<sub>3</sub>C<sub>6</sub>H<sub>2</sub>NC<sub>3</sub>H<sub>2</sub>NCH<sub>2</sub>CH<sub>2</sub>NH-2,4,6-Me<sub>3</sub>C<sub>6</sub>H<sub>2</sub>)Ru(CHPh)(PCy<sub>3</sub>)Cl<sub>2</sub>]

[(2,4,6-Me3C6H2NC3H2NCH2CH2NH-2,4,6-Me3C6H2)Ru(CHPh)(PCy3)Cl2]

Guidance literature:
In toluene; byproducts: P(C6H11)3; (N2); Schlenk technique; soln. of ligand (1 equiv.) in toluene was addedto soln. of Ru complex in toluene; stirred overnight; concd. (vac.); hexane added; filtered; washed (hexane); elem. anal.;
DOI:10.1021/om2000844
upstream raw materials:

1-(2,4,6-trimethylphenyl)-3-(2-((2,4,6-trimethylphenyl)amino)ethyl)imidazolium chloride

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