N-(4-n-butylphenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzenamine

Base Information

Chemical Name:N-(4-n-butylphenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzenamine
CAS No.:1383601-98-6
Molecular Formula:C₂₈H₃₄BNO₂
Molecular Weight:427.394
Hs Code.:

Synonyms:N-(4-n-butylphenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzenamine

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Chemical Property of N-(4-n-butylphenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzenamine

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Technology Process of N-(4-n-butylphenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzenamine

There total 4 articles about N-(4-n-butylphenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 230623-63-9
N-(4-bromophenyl)-N-(4-n-butylphenyl)benzenamine

: 1383601-98-6
N-(4-n-butylphenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzenamine

Guidance literature:: N-(4-bromophenyl)-N-(4-n-butylphenyl)benzenamine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 2h; Inert atmosphere;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 26h; Inert atmosphere;
DOI:10.1016/j.polymer.2012.05.011

Reference yield:

: 152270-84-3
N-(4-n-butylphenyl)-N-phenylbenzenamine

: 1383601-98-6
N-(4-n-butylphenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzenamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

2.2: 26 h / -78 - 20 °C / Inert atmosphere

With N-Bromosuccinimide; n-butyllithium; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1016/j.polymer.2012.05.011

Reference yield:

: 41492-05-1
p-bromobutylbenzene

: 1383601-98-6
N-(4-n-butylphenyl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzenamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate / hexane; toluene / 16 h / Inert atmosphere; Reflux

2.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

3.2: 26 h / -78 - 20 °C / Inert atmosphere

With N-Bromosuccinimide; n-butyllithium; tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.polymer.2012.05.011