C₂₅H₃₂O₃SSe

Base Information

• Chemical Name: C₂₅H₃₂O₃SSe
• CAS No.: 137792-20-2
• Molecular Formula: C₂₅H₃₂O₃SSe
• Molecular Weight: 491.553
• Mol file: 137792-20-2.mol

Synonyms:C₂₅H₃₂O₃SSe

Chemical Property of C₂₅H₃₂O₃SSe

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₂₅H₃₂O₃SSe

There total 4 articles about C₂₅H₃₂O₃SSe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

iodo(phenylseleno)methane (153908-42-0) → C25H32O3SSe (137792-20-2)

Guidance literature:

Multi-step reaction with 2 steps

1: NaH / dimethylformamide

2: 1.) PPTs / 1.) 25 deg C, 2 h, 2.) THF, H₂O

With pyridinium p-toluenesulfonate; sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1021/ja00026a030

Reference yield:

1β,2,3,4,4a,5,8,9,10,10aα-decahydro-4aβ-(mercaptomethyl)-7-methoxy-1α-methyl-2-phenanthrone 2-(ethylene acetal) (105619-51-0) → C25H32O3SSe (137792-20-2)

Guidance literature:

Multi-step reaction with 2 steps

1: NaH / dimethylformamide

2: 1.) PPTs / 1.) 25 deg C, 2 h, 2.) THF, H₂O

With pyridinium p-toluenesulfonate; sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1021/ja00026a030

Reference yield:

C26H34O3SSe → C25H32O3SSe (137720-65-1) + C25H32O3SSe (137720-64-0) + C25H32O3SSe (137792-20-2)

Guidance literature:

With pyridinium p-toluenesulfonate; Yield given. Multistep reaction. Yields of byproduct given; 1.) 25 deg C, 2 h, 2.) THF, H₂O;

DOI:10.1021/ja00026a030

upstream raw materials:

iodo(phenylseleno)methane

1β,2,3,4,4a,5,8,9,10,10aα-decahydro-4aβ-(mercaptomethyl)-7-methoxy-1α-methyl-2-phenanthrone 2-(ethylene acetal)