1-[4-[[aminoacetyl]amino]phenyl]-4-carboxy-5,8,11-tris(carboxymethyl)-2-oxa-5,8,11-triazatridecan-13-oic acid

Base Information

Chemical Name:1-[4-[[aminoacetyl]amino]phenyl]-4-carboxy-5,8,11-tris(carboxymethyl)-2-oxa-5,8,11-triazatridecan-13-oic acid
CAS No.:731009-35-1
Molecular Formula:C₂₄H₃₅N₅O₁₂
Molecular Weight:585.568
Hs Code.:

Synonyms:1-[4-[[aminoacetyl]amino]phenyl]-4-carboxy-5,8,11-tris(carboxymethyl)-2-oxa-5,8,11-triazatridecan-13-oic acid

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Chemical Property of 1-[4-[[aminoacetyl]amino]phenyl]-4-carboxy-5,8,11-tris(carboxymethyl)-2-oxa-5,8,11-triazatridecan-13-oic acid

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Technology Process of 1-[4-[[aminoacetyl]amino]phenyl]-4-carboxy-5,8,11-tris(carboxymethyl)-2-oxa-5,8,11-triazatridecan-13-oic acid

There total 3 articles about 1-[4-[[aminoacetyl]amino]phenyl]-4-carboxy-5,8,11-tris(carboxymethyl)-2-oxa-5,8,11-triazatridecan-13-oic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 174267-44-8
5-[[(4-[[[[(1,1-dimethylethoxy)carbonyl]amino]acetyl]amino]phenyl)methoxy]methyl]-6,9,12-tris[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

: 731009-35-1
1-[4-[[aminoacetyl]amino]phenyl]-4-carboxy-5,8,11-tris(carboxymethyl)-2-oxa-5,8,11-triazatridecan-13-oic acid

Guidance literature:: With methoxybenzene; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 72h;
DOI:10.1021/jm0310683

Reference yield:

: 174267-42-6
6,9,12-tris[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-5-[[(4-nitrophenyl)methoxy]methyl]-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

: 731009-35-1
1-[4-[[aminoacetyl]amino]phenyl]-4-carboxy-5,8,11-tris(carboxymethyl)-2-oxa-5,8,11-triazatridecan-13-oic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / H₂ / Pd/C / ethanol / 1 h / 20 °C

2: 51 percent / diethyl cyanophosphonate; Et₃N / dimethylformamide / 16 h / 0 °C

3: trifluoroacetic acid; anisole / CH₂Cl₂ / 72 h / 20 °C

With diethyl cyanophosphonate; hydrogen; methoxybenzene; triethylamine; trifluoroacetic acid; palladium on activated charcoal; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0310683

Reference yield:

: 174267-43-7
5-[[(4-aminophenyl)methoxy]methyl]-6,9,12-tris[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

: 731009-35-1
1-[4-[[aminoacetyl]amino]phenyl]-4-carboxy-5,8,11-tris(carboxymethyl)-2-oxa-5,8,11-triazatridecan-13-oic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / diethyl cyanophosphonate; Et₃N / dimethylformamide / 16 h / 0 °C

2: trifluoroacetic acid; anisole / CH₂Cl₂ / 72 h / 20 °C

With diethyl cyanophosphonate; methoxybenzene; triethylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0310683