5-[[(4-aminophenyl)methoxy]methyl]-6,9,12-tris[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

Base Information

Chemical Name:5-[[(4-aminophenyl)methoxy]methyl]-6,9,12-tris[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester
CAS No.:174267-43-7
Molecular Formula:C₄₂H₇₂N₄O₁₁
Molecular Weight:809.054
Hs Code.:

5-[[(4-aminophenyl)methoxy]methyl]-6,9,12-tris[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

Synonyms:5-[[(4-aminophenyl)methoxy]methyl]-6,9,12-tris[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

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Chemical Property of 5-[[(4-aminophenyl)methoxy]methyl]-6,9,12-tris[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

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Technology Process of 5-[[(4-aminophenyl)methoxy]methyl]-6,9,12-tris[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

There total 1 articles about 5-[[(4-aminophenyl)methoxy]methyl]-6,9,12-tris[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 174267-42-6
6,9,12-tris[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-5-[[(4-nitrophenyl)methoxy]methyl]-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

: 174267-43-7
5-[[(4-aminophenyl)methoxy]methyl]-6,9,12-tris[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 20 ℃; for 1h;
DOI:10.1021/jm0310683

Reference yield: 51.0%

: 4530-20-5
BOC-glycine

: 174267-43-7
5-[[(4-aminophenyl)methoxy]methyl]-6,9,12-tris[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

: 174267-44-8
5-[[(4-[[[[(1,1-dimethylethoxy)carbonyl]amino]acetyl]amino]phenyl)methoxy]methyl]-6,9,12-tris[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

Guidance literature:: With diethyl cyanophosphonate; triethylamine; In N,N-dimethyl-formamide; at 0 ℃; for 16h;
DOI:10.1021/jm0310683

Reference yield:

: 174267-43-7
5-[[(4-aminophenyl)methoxy]methyl]-6,9,12-tris[2-(1,1-dimethylethoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oic acid 1,1-dimethylethyl ester

: 731009-35-1
1-[4-[[aminoacetyl]amino]phenyl]-4-carboxy-5,8,11-tris(carboxymethyl)-2-oxa-5,8,11-triazatridecan-13-oic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / diethyl cyanophosphonate; Et₃N / dimethylformamide / 16 h / 0 °C

2: trifluoroacetic acid; anisole / CH₂Cl₂ / 72 h / 20 °C

With diethyl cyanophosphonate; methoxybenzene; triethylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0310683