(2S,3R)-3-Benzenesulfonyl-5-(1-phenylselanyl-ethyl)-2-tridecyl-tetrahydro-furan

Base Information

Chemical Name:(2S,3R)-3-Benzenesulfonyl-5-(1-phenylselanyl-ethyl)-2-tridecyl-tetrahydro-furan
CAS No.:111533-68-7
Molecular Formula:C₃₁H₄₆O₃SSe
Molecular Weight:577.73
Hs Code.:

Synonyms:(2S,3R)-3-Benzenesulfonyl-5-(1-phenylselanyl-ethyl)-2-tridecyl-tetrahydro-furan

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-3-Benzenesulfonyl-5-(1-phenylselanyl-ethyl)-2-tridecyl-tetrahydro-furan

Chemical Property:

Purity/Quality:

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Technology Process of (2S,3R)-3-Benzenesulfonyl-5-(1-phenylselanyl-ethyl)-2-tridecyl-tetrahydro-furan

There total 7 articles about (2S,3R)-3-Benzenesulfonyl-5-(1-phenylselanyl-ethyl)-2-tridecyl-tetrahydro-furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 5707-04-0
Phenylselenyl chloride

: 111533-56-3,111533-57-4
(5R,6S)-5-phenylsulphonylnonadec-2-en-6-ol

: 111533-68-7
(2S,3R)-3-Benzenesulfonyl-5-(1-phenylselanyl-ethyl)-2-tridecyl-tetrahydro-furan

Guidance literature:: In dichloromethane; at -78 ℃; for 1h;

Reference yield:

: 23886-96-6
1-chloro-3-phenylsulphonylpropane-2-one

: 111533-68-7
(2S,3R)-3-Benzenesulfonyl-5-(1-phenylselanyl-ethyl)-2-tridecyl-tetrahydro-furan

Guidance literature:: Multi-step reaction with 5 steps

1: 63 percent / baker's yeast, sucrose / H₂O / 48 h / 20 °C

2: 84 percent / silver(I) oxide / 1,2-dimethoxy-ethane / 60 h / 85 °C

3: 72 percent / copper(I) iodide / diethyl ether; tetrahydrofuran / 0.08 h / -60 °C

4: 1.) butyl-lithium / 1.) hexane, THF, -78 deg C, 30 min; 2.) hexane, THF, r.t., 30 min

5: 88 percent / CH₂Cl₂ / 1 h / -78 °C

With copper(l) iodide; n-butyllithium; baker's yeast; silver(l) oxide; Sucrose; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; dichloromethane; water;

Reference yield:

: 22198-54-5
1-chloro-3-phenylsulfanylpropan-2-one

: 111533-68-7
(2S,3R)-3-Benzenesulfonyl-5-(1-phenylselanyl-ethyl)-2-tridecyl-tetrahydro-furan

Guidance literature:: Multi-step reaction with 6 steps

1: MCPBA / CHCl₃ / 30 h / Ambient temperature

2: 63 percent / baker's yeast, sucrose / H₂O / 48 h / 20 °C

3: 84 percent / silver(I) oxide / 1,2-dimethoxy-ethane / 60 h / 85 °C

4: 72 percent / copper(I) iodide / diethyl ether; tetrahydrofuran / 0.08 h / -60 °C

5: 1.) butyl-lithium / 1.) hexane, THF, -78 deg C, 30 min; 2.) hexane, THF, r.t., 30 min

6: 88 percent / CH₂Cl₂ / 1 h / -78 °C

With copper(l) iodide; n-butyllithium; baker's yeast; 3-chloro-benzenecarboperoxoic acid; silver(l) oxide; Sucrose; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; dichloromethane; chloroform; water;