N--L-norleucine

Base Information

Chemical Name:N--L-norleucine
CAS No.:118586-12-2
Molecular Formula:C₂₇H₃₀N₂O₅
Molecular Weight:462.546
Hs Code.:

N-<N-benzyloxycarbonyl-3-(1-naphthyl)-L-alanyl>-L-norleucine

Synonyms:N--L-norleucine

Suppliers and Price of N--L-norleucine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N--L-norleucine

Chemical Property:

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Technology Process of N--L-norleucine

There total 4 articles about N--L-norleucine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 141714-15-0
(S)-methyl 2-((S)-2-(((benzyloxy)carbonyl)amino)-3-(naphthalen-1-yl)propanamido)hexanoate

: 118586-12-2
N--L-norleucine

Guidance literature:: With potassium hydroxide; In ethanol; water; Ambient temperature;
DOI:10.1248/cpb.40.364

Reference yield:

: 59759-78-3
2-benzoylamino-3-naphthalen-1-yl-propionic acid

: 118586-12-2
N--L-norleucine

Guidance literature:: Multi-step reaction with 4 steps

1: 87.6 percent / aq. NaOH, phosphate buffer / 25 h / 37 °C / acylase from Streptoverticillium rimofaciens

2: 94 percent / 1 N aq. NaOH / 1.67 h / 0 °C

3: 84.5 percent / N-methylmorpholine, HOBT, DCC / 3 h / -5 °C

4: 98 percent / KOH / ethanol; H₂O / Ambient temperature

With 4-methyl-morpholine; potassium hydroxide; sodium hydroxide; phosphate buffer; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In ethanol; water;
DOI:10.1248/cpb.40.364

Reference yield:

: 55516-54-6,68798-79-8,7758-42-1
L-1-naphthylalanine

: 118586-12-2
N--L-norleucine

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / 1 N aq. NaOH / 1.67 h / 0 °C

2: 84.5 percent / N-methylmorpholine, HOBT, DCC / 3 h / -5 °C

3: 98 percent / KOH / ethanol; H₂O / Ambient temperature

With 4-methyl-morpholine; potassium hydroxide; sodium hydroxide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In ethanol; water;
DOI:10.1248/cpb.40.364