benzyl O-(2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl)-(1->4)-2,3-di-O-benzyl-6-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:benzyl O-(2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl)-(1->4)-2,3-di-O-benzyl-6-deoxy-β-D-glucopyranoside
CAS No.:279678-06-7
Molecular Formula:C₄₇H₅₂O₉
Molecular Weight:760.924
Hs Code.:

Synonyms:benzyl O-(2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl)-(1->4)-2,3-di-O-benzyl-6-deoxy-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl O-(2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl)-(1->4)-2,3-di-O-benzyl-6-deoxy-β-D-glucopyranoside

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Technology Process of benzyl O-(2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl)-(1->4)-2,3-di-O-benzyl-6-deoxy-β-D-glucopyranoside

There total 9 articles about benzyl O-(2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl)-(1->4)-2,3-di-O-benzyl-6-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 107-18-6
allyl alcohol

: 279678-14-7
benzyl O-(4-O-allyl-2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl)-(1->4)-2,3-di-O-benzyl-6-deoxy-β-D-glucopyranoside

: 279678-06-7
benzyl O-(2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl)-(1->4)-2,3-di-O-benzyl-6-deoxy-β-D-glucopyranoside

Guidance literature:: With sodium acetate; palladium dichloride; In water; acetic acid; at 20 ℃; for 16h;
DOI:10.1246/bcsj.73.967

Reference yield: 70.0%

: 279678-20-5
benzyl O-(2,3-di-O-benzyl-6-O-tosyl-α-D-glucopyranosyl)-(1->4)-2,3-di-O-benzyl-6-O-tosyl-β-D-glucopyranoside

: 279678-06-7
benzyl O-(2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl)-(1->4)-2,3-di-O-benzyl-6-deoxy-β-D-glucopyranoside

Guidance literature:: With lithium aluminium tetrahydride; at 50 ℃; for 0.5h;
DOI:10.1246/bcsj.73.967

Reference yield:

: 30607-98-8,35905-28-3,40983-94-6,56341-65-2,57783-86-5,58006-32-9,72869-10-4,73366-72-0,79549-73-8,110850-30-1,113973-86-7,117895-05-3
benzyl 4,6-O-benzylidene-β-D-glucopyranoside

: 279678-06-7
benzyl O-(2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl)-(1->4)-2,3-di-O-benzyl-6-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 81 percent / KOH / 1.3 h / 120 °C

2: 74 percent / pyridine / 72 h / 0 - 20 °C

3: 71 percent / LiAlH₄ / diethyl ether / 0.83 h / 50 °C

4: p-NO₂C₆H₄SO₂Cl; AgOTf; Et₃N / CH₂Cl₂ / 18 h / -60 - 0 °C

5: 84 percent / NaOAc; PdCl₂ / acetic acid; H₂O / 16 h / 20 °C

With potassium hydroxide; lithium aluminium tetrahydride; sodium acetate; silver trifluoromethanesulfonate; triethylamine; 4-Nitrobenzenesulfonyl chloride; palladium dichloride; In pyridine; diethyl ether; dichloromethane; water; acetic acid; 1: Ring cleavage / 2: Tosylation / 3: Hydrogenolysis / 4: Condensation / 5: Substitution;
DOI:10.1246/bcsj.73.967