C₂₈H₂₇BrO₂

Base Information

Chemical Name:C₂₈H₂₇BrO₂
CAS No.:1313396-52-9
Molecular Formula:C₂₈H₂₇BrO₂
Molecular Weight:475.425
Hs Code.:

C<sub>28</sub>H<sub>27</sub>BrO<sub>2</sub>

Synonyms:C₂₈H₂₇BrO₂

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Chemical Property of C₂₈H₂₇BrO₂

Chemical Property:

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Technology Process of C₂₈H₂₇BrO₂

There total 4 articles about C₂₈H₂₇BrO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1210959-87-7
4-(2-(2,2-diphenylvinylidene)-1-(4-methoxyphenyl)cyclopropyl)butan-1-ol

: 1313396-52-9
C₂₈H₂₇BrO₂

Guidance literature:: With N-Bromosuccinimide; sodium hydrogencarbonate; In acetonitrile; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1055/s-0030-1259715

Reference yield:

: 530-48-3
1,1-Diphenylethylene

: 1313396-52-9
C₂₈H₂₇BrO₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium tert-butylate / pentane

2.1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / tetrahydrofuran / 36 h / 20 °C

3.1: diborane / tetrahydrofuran / 0 °C

3.2: 0 °C

4.1: N-Bromosuccinimide; sodium hydrogencarbonate / acetonitrile / 3 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; potassium tert-butylate; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; sodium hydroxide; diborane; In tetrahydrofuran; acetonitrile; pentane;
DOI:10.1055/s-0030-1259715

Reference yield:

: 1201909-52-5
1-(1-(but-3-enyl)-2-(2,2-diphenylvinylidene)cyclopropyl)-4-methoxybenzene

: 1313396-52-9
C₂₈H₂₇BrO₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: diborane / tetrahydrofuran / 0 °C

1.2: 0 °C

2.1: N-Bromosuccinimide; sodium hydrogencarbonate / acetonitrile / 3 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; sodium hydrogencarbonate; diborane; In tetrahydrofuran; acetonitrile;
DOI:10.1055/s-0030-1259715