(E)-1-(2-bromo-4,5-dimethoxyphenyl)-2-(2-bromophenyl)-N,N-dimethylethenylamine

Base Information

Chemical Name:(E)-1-(2-bromo-4,5-dimethoxyphenyl)-2-(2-bromophenyl)-N,N-dimethylethenylamine
CAS No.:299215-73-9
Molecular Formula:C₁₈H₁₉Br₂NO₂
Molecular Weight:441.162
Hs Code.:

Synonyms:(E)-1-(2-bromo-4,5-dimethoxyphenyl)-2-(2-bromophenyl)-N,N-dimethylethenylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-(2-bromo-4,5-dimethoxyphenyl)-2-(2-bromophenyl)-N,N-dimethylethenylamine

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Technology Process of (E)-1-(2-bromo-4,5-dimethoxyphenyl)-2-(2-bromophenyl)-N,N-dimethylethenylamine

There total 3 articles about (E)-1-(2-bromo-4,5-dimethoxyphenyl)-2-(2-bromophenyl)-N,N-dimethylethenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 578-51-8
2-bromobenzylchloride

: 193557-58-3
2-(2-bromo-4,5-dimethoxyphenyl)-2-(N,N-dimethylamino)acetonitrile

: 299215-73-9
(E)-1-(2-bromo-4,5-dimethoxyphenyl)-2-(2-bromophenyl)-N,N-dimethylethenylamine

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at -19 - 20 ℃;
DOI:10.1021/jo0002700

Reference yield:

: 5392-10-9
2-bromo-4,5-dimethoxybenzaldehyde

: 299215-73-9
(E)-1-(2-bromo-4,5-dimethoxyphenyl)-2-(2-bromophenyl)-N,N-dimethylethenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / acetonitrile; H₂O / 48 h / 20 °C

2: 80 percent / NaH / dimethylformamide / -19 - 20 °C

With sodium hydride; In water; N,N-dimethyl-formamide; acetonitrile; 1: Addition / 2: Alkylation;
DOI:10.1021/jo0002700

Reference yield:

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 299215-73-9
(E)-1-(2-bromo-4,5-dimethoxyphenyl)-2-(2-bromophenyl)-N,N-dimethylethenylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / Br₂ / CHCl₃ / 6 h / 60 °C

2: 89 percent / acetonitrile; H₂O / 48 h / 20 °C

3: 80 percent / NaH / dimethylformamide / -19 - 20 °C

With bromine; sodium hydride; In chloroform; water; N,N-dimethyl-formamide; acetonitrile; 1: Bromination / 2: Addition / 3: Alkylation;
DOI:10.1021/jo0002700