4-bromo-5-butyl-2-hydroxymethyl-N,N'-bis{[2'-[2-(trityl)tetrazol-5-yl]biphenyl-4-yl]methyl}imidazolium bromide

Base Information

• Chemical Name: 4-bromo-5-butyl-2-hydroxymethyl-N,N'-bis{[2'-[2-(trityl)tetrazol-5-yl]biphenyl-4-yl]methyl}imidazolium bromide
• CAS No.: 1431152-63-4
• Molecular Formula: Br*C₇₄H₆₂BrN₁₀O
• Molecular Weight: 1267.18

Synonyms:4-bromo-5-butyl-2-hydroxymethyl-N,N'-bis{[2'-[2-(trityl)tetrazol-5-yl]biphenyl-4-yl]methyl}imidazolium bromide

Chemical Property of 4-bromo-5-butyl-2-hydroxymethyl-N,N'-bis{[2'-[2-(trityl)tetrazol-5-yl]biphenyl-4-yl]methyl}imidazolium bromide

Chemical Property:

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Technology Process of 4-bromo-5-butyl-2-hydroxymethyl-N,N'-bis{[2'-[2-(trityl)tetrazol-5-yl]biphenyl-4-yl]methyl}imidazolium bromide

There total 1 articles about 4-bromo-5-butyl-2-hydroxymethyl-N,N'-bis{[2'-[2-(trityl)tetrazol-5-yl]biphenyl-4-yl]methyl}imidazolium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 4-bromo-5-butyl-N,N'-bis{[2'-[2-(trityl)tetrazol-5-yl]biphenyl-4-yl]methyl}imidazolium bromide (1431152-49-6) → 4-bromo-5-butyl-2-hydroxymethyl-N,N'-bis{[2'-[2-(trityl)tetrazol-5-yl]biphenyl-4-yl]methyl}imidazolium bromide (1431152-63-4)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 80 ℃; for 1h; Sealed tube;

DOI:10.1016/j.ejmech.2012.12.044

Reference yield: 77.0%

4-bromo-5-butyl-2-hydroxymethyl-N,N'-bis{[2'-[2-(trityl)tetrazol-5-yl]biphenyl-4-yl]methyl}imidazolium bromide (1431152-63-4) → C36H34BrN10O(1+)*Br(1-) (1431152-69-0)

Guidance literature:

With triethylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1016/j.ejmech.2012.12.044

upstream raw materials:

formaldehyd

4-bromo-5-butyl-N,N'-bis{[2'-[2-(trityl)tetrazol-5-yl]biphenyl-4-yl]methyl}imidazolium bromide

Downstream raw materials:

C₃₆H₃₄BrN₁₀O⁽¹⁺⁾*Br^(1-)

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