mer-trans-Mo(CO)3(P(C₆H₁₁)3)2(H₂)

Base Information

• Chemical Name: mer-trans-Mo(CO)3(P(C₆H₁₁)3)2(H₂)
• CAS No.: 88211-52-3
• Molecular Formula: C₃₉H₆₈MoO₃P₂
• Molecular Weight: 742.855
• Mol file: 88211-52-3.mol

Synonyms:mer-trans-Mo(CO)3(P(C₆H₁₁)3)2(H₂)

Chemical Property of mer-trans-Mo(CO)3(P(C₆H₁₁)3)2(H₂)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of mer-trans-Mo(CO)3(P(C₆H₁₁)3)2(H₂)

There total 2 articles about mer-trans-Mo(CO)3(P(C₆H₁₁)3)2(H₂) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

tricarbonyl(cycloheptatriene)molybdenum(0) (121719-12-8,12125-77-8) + tricyclohexylphosphine (2622-14-2) → mer-trans-Mo(CO)3(P(C6H11)3)2(H2) (88211-52-3)

Guidance literature:

With hydrogen; In toluene; byproducts: cycloheptatriene; (H2 or Ar), mixture stirred under H2 for 30 min; product collected, washed with heptane/toluene 2:1, dried in H2, elem. anal.;

DOI:10.1021/ja00282a026

Reference yield:

[Mo(tricyclohexylphosphine)2(CO)3] (73690-53-6) → mer-trans-Mo(CO)3(P(C6H11)3)2(H2) (88211-52-3)

Guidance literature:

With hydrogen; In toluene; H2 addn.; product collected, washed with heptane/toluene 2:1, dried in H2;

DOI:10.1021/ja00282a026

Reference yield:

mer-trans-Mo(CO)3(P(C6H11)3)2(H2) (88211-52-3) → [Mo(tricyclohexylphosphine)2(CO)3] (73690-53-6)

Guidance literature:

In toluene; byproducts: H2; (H2 or Ar), slurry heated to reflux;

DOI:10.1021/ja00282a026

upstream raw materials:

[Mo(tricyclohexylphosphine)2(CO)3]

tricarbonyl(cycloheptatriene)molybdenum⁽⁰⁾

tricyclohexylphosphine

Downstream raw materials:

[Mo(tricyclohexylphosphine)2(CO)3]

Mo(CO)3(P(C₆H₁₁)3)2

Refernces