10-deacetyl-7,10-bis<<(2,2,2-trichloroethyl)oxy>carbonyl>-1a'-homotaxol

Base Information

Chemical Name:10-deacetyl-7,10-bis<<(2,2,2-trichloroethyl)oxy>carbonyl>-1a'-homotaxol
CAS No.:160237-92-3
Molecular Formula:C₅₂H₅₃Cl₆NO₁₇
Molecular Weight:1176.71
Hs Code.:

Synonyms:10-deacetyl-7,10-bis<<(2,2,2-trichloroethyl)oxy>carbonyl>-1a'-homotaxol

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Chemical Property of 10-deacetyl-7,10-bis<<(2,2,2-trichloroethyl)oxy>carbonyl>-1a'-homotaxol

Chemical Property:

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Technology Process of 10-deacetyl-7,10-bis<<(2,2,2-trichloroethyl)oxy>carbonyl>-1a'-homotaxol

There total 4 articles about 10-deacetyl-7,10-bis<<(2,2,2-trichloroethyl)oxy>carbonyl>-1a'-homotaxol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 98-88-4
benzoyl chloride

: 160237-91-2
10-deacetyl-3'-N-debenzoyl-7,10-bis<<(2,2,2-trichloroethyl)oxy>carbonyl>-1a'-homotaxol

: 160237-92-3
10-deacetyl-7,10-bis<<(2,2,2-trichloroethyl)oxy>carbonyl>-1a'-homotaxol

Guidance literature:: With sodium hydrogencarbonate; In water; ethyl acetate; for 0.333333h; Ambient temperature;

Reference yield:

: 95603-44-4
7,10-di-(2,2,2-trichloroethyloxycarbonyl)-10-deacetylbaccatin III

: 160237-92-3
10-deacetyl-7,10-bis<<(2,2,2-trichloroethyl)oxy>carbonyl>-1a'-homotaxol

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / DCC, DMAP / toluene / 2 h / 80 °C

2: 73 percent / 90percent formic acid / 4 h / Ambient temperature

3: 79 percent / NaHCO₃ / ethyl acetate; H₂O / 0.33 h / Ambient temperature

With dmap; formic acid; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In water; ethyl acetate; toluene;

Reference yield:

: 160237-89-8
(4S,5S)-3-(tert-butoxycarbonyl)-2,2-dimethyl-4-phenyl-1,3-oxazolidine-5-acetic acid

: 160237-92-3
10-deacetyl-7,10-bis<<(2,2,2-trichloroethyl)oxy>carbonyl>-1a'-homotaxol

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / DCC, DMAP / toluene / 2 h / 80 °C

2: 73 percent / 90percent formic acid / 4 h / Ambient temperature

3: 79 percent / NaHCO₃ / ethyl acetate; H₂O / 0.33 h / Ambient temperature

With dmap; formic acid; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In water; ethyl acetate; toluene;