tert-butyl (1S,2S)-1-(methoxycarbonyl)-2-acetoxy-4-(benzyloxy)butylcarbamate

Base Information

Chemical Name:tert-butyl (1S,2S)-1-(methoxycarbonyl)-2-acetoxy-4-(benzyloxy)butylcarbamate
CAS No.:1383178-67-3
Molecular Formula:C₂₀H₂₉NO₇
Molecular Weight:395.453
Hs Code.:

Synonyms:tert-butyl (1S,2S)-1-(methoxycarbonyl)-2-acetoxy-4-(benzyloxy)butylcarbamate

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Chemical Property of tert-butyl (1S,2S)-1-(methoxycarbonyl)-2-acetoxy-4-(benzyloxy)butylcarbamate

Chemical Property:

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Technology Process of tert-butyl (1S,2S)-1-(methoxycarbonyl)-2-acetoxy-4-(benzyloxy)butylcarbamate

There total 5 articles about tert-butyl (1S,2S)-1-(methoxycarbonyl)-2-acetoxy-4-(benzyloxy)butylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1383178-53-7
tert-butyl (1S,2S)-1-(methoxycarbonyl)-4-(benzyloxy)-2-hydroxybutylcarbamate

: 108-24-7
acetic anhydride

: 1383178-67-3
tert-butyl (1S,2S)-1-(methoxycarbonyl)-2-acetoxy-4-(benzyloxy)butylcarbamate

Guidance literature:: With dmap; triethylamine; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1016/j.molcatb.2011.11.004

Reference yield:

: 1383178-38-8
tert-butyl (S)-1-(methoxycarbonyl)-4-(benzyloxy)-2-hydroxybutylcarbamate

: 108-24-7
acetic anhydride

: 1383178-50-4
tert-butyl (1R,2S)-1-(methoxycarbonyl)-2-acetoxy-4-(benzyloxy)butylcarbamate

: 1383178-67-3
tert-butyl (1S,2S)-1-(methoxycarbonyl)-2-acetoxy-4-(benzyloxy)butylcarbamate

Guidance literature:: With dmap; triethylamine; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1016/j.molcatb.2011.11.004

Reference yield:

: 1383178-38-8
tert-butyl (S)-1-(methoxycarbonyl)-4-(benzyloxy)-2-hydroxybutylcarbamate

: 1383178-67-3
tert-butyl (1S,2S)-1-(methoxycarbonyl)-2-acetoxy-4-(benzyloxy)butylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: immobilised lipase from Pseudomonas / tert-butyl methyl ether / 96 h / 45 °C / Enzymatic reaction

2: dmap; triethylamine / tetrahydrofuran / 24 h / 20 °C

With dmap; triethylamine; In tetrahydrofuran; tert-butyl methyl ether;
DOI:10.1016/j.molcatb.2011.11.004