tert-butyl (1S,2S)-1-(methoxycarbonyl)-4-(benzyloxy)-2-hydroxybutylcarbamate

Base Information

Chemical Name:tert-butyl (1S,2S)-1-(methoxycarbonyl)-4-(benzyloxy)-2-hydroxybutylcarbamate
CAS No.:1383178-53-7
Molecular Formula:C₁₈H₂₇NO₆
Molecular Weight:353.415
Hs Code.:

Synonyms:tert-butyl (1S,2S)-1-(methoxycarbonyl)-4-(benzyloxy)-2-hydroxybutylcarbamate

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Chemical Property of tert-butyl (1S,2S)-1-(methoxycarbonyl)-4-(benzyloxy)-2-hydroxybutylcarbamate

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Technology Process of tert-butyl (1S,2S)-1-(methoxycarbonyl)-4-(benzyloxy)-2-hydroxybutylcarbamate

There total 3 articles about tert-butyl (1S,2S)-1-(methoxycarbonyl)-4-(benzyloxy)-2-hydroxybutylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 108-05-4,9003-20-7
vinyl acetate

: 1383178-38-8
tert-butyl (S)-1-(methoxycarbonyl)-4-(benzyloxy)-2-hydroxybutylcarbamate

: 1383178-53-7
tert-butyl (1S,2S)-1-(methoxycarbonyl)-4-(benzyloxy)-2-hydroxybutylcarbamate

: 1383178-50-4
tert-butyl (1R,2S)-1-(methoxycarbonyl)-2-acetoxy-4-(benzyloxy)butylcarbamate

Guidance literature:: With immobilised lipase from Pseudomonas; In tert-butyl methyl ether; at 45 ℃; for 96h; optical yield given as %ee; Enzymatic reaction;
DOI:10.1016/j.molcatb.2011.11.004

Reference yield:

: (2S)-2-amino-5-(benzyloxy)-3-hydroxypentanoic acid

: 1383178-53-7
tert-butyl (1S,2S)-1-(methoxycarbonyl)-4-(benzyloxy)-2-hydroxybutylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 12 h / 0 - 20 °C / Inert atmosphere

2: water; ethyl acetate / 12 h / 0 - 20 °C

With thionyl chloride; In water; ethyl acetate;
DOI:10.1016/j.molcatb.2011.11.004