sodium [6-[(4-fluoro-phenyl)-carbonyl]-2,1,3-benzothiadiazole-5-yl]-methanesulfonate

Base Information

Chemical Name:sodium [6-[(4-fluoro-phenyl)-carbonyl]-2,1,3-benzothiadiazole-5-yl]-methanesulfonate
CAS No.:1282510-22-8
Molecular Formula:C₁₄H₈FN₂O₄S₂*Na
Molecular Weight:374.349
Hs Code.:

Synonyms:sodium [6-[(4-fluoro-phenyl)-carbonyl]-2,1,3-benzothiadiazole-5-yl]-methanesulfonate

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Chemical Property of sodium [6-[(4-fluoro-phenyl)-carbonyl]-2,1,3-benzothiadiazole-5-yl]-methanesulfonate

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Technology Process of sodium [6-[(4-fluoro-phenyl)-carbonyl]-2,1,3-benzothiadiazole-5-yl]-methanesulfonate

There total 3 articles about sodium [6-[(4-fluoro-phenyl)-carbonyl]-2,1,3-benzothiadiazole-5-yl]-methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: [6-(chloromethyl)-2,1,3-benzothiadiazol-5-yl](4-fluorophenyl)methanone

: 1282510-22-8
sodium [6-[(4-fluoro-phenyl)-carbonyl]-2,1,3-benzothiadiazole-5-yl]-methanesulfonate

Guidance literature:: With sodium sulfite; In 1,4-dioxane; water; for 2h; Reflux;
DOI:10.1002/jhet.2141

Reference yield:

: 1376450-72-4
5H,7H-furo[3,4-f][2,1,3]benzothiadiazol-5-one

: 1282510-22-8
sodium [6-[(4-fluoro-phenyl)-carbonyl]-2,1,3-benzothiadiazole-5-yl]-methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride; boron trifluoride diethyl etherate; N-benzyl-N,N,N-triethylammonium chloride / 5,5-dimethyl-1,3-cyclohexadiene / 5 h / Reflux

2: aluminum (III) chloride / dichloromethane / 2 h / 0 - 20 °C

3: sodium sulfite / water; 1,4-dioxane / 2 h / Reflux

With aluminum (III) chloride; thionyl chloride; boron trifluoride diethyl etherate; N-benzyl-N,N,N-triethylammonium chloride; sodium sulfite; In 1,4-dioxane; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; water;
DOI:10.1002/jhet.2141

Reference yield:

: 6-(chloromethyl)-2,1,3-benzothiadiazole-5-carbonyl chloride

: 1282510-22-8
sodium [6-[(4-fluoro-phenyl)-carbonyl]-2,1,3-benzothiadiazole-5-yl]-methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride / dichloromethane / 2 h / 0 - 20 °C

2: sodium sulfite / water; 1,4-dioxane / 2 h / Reflux

With aluminum (III) chloride; sodium sulfite; In 1,4-dioxane; dichloromethane; water;
DOI:10.1002/jhet.2141