(C₅(CH₃)5)Ru(CO)2(P(CH₃)2C₆H₅)⁽¹⁺⁾*I^(1-)=(C₅(CH₃)5)Ru(CO)2(P(CH₃)2C₆H₅)⁽¹⁺⁾I^(1-)

Base Information

• Chemical Name: (C₅(CH₃)5)Ru(CO)2(P(CH₃)2C₆H₅)⁽¹⁺⁾*I^(1-)=(C₅(CH₃)5)Ru(CO)2(P(CH₃)2C₆H₅)⁽¹⁺⁾I^(1-)
• CAS No.: 88296-33-7
• Molecular Formula: C₂₀H₂₆O₂PRu*I
• Molecular Weight: 557.373

Synonyms:(C₅(CH₃)5)Ru(CO)2(P(CH₃)2C₆H₅)⁽¹⁺⁾*I^(1-)=(C₅(CH₃)5)Ru(CO)2(P(CH₃)2C₆H₅)⁽¹⁺⁾I^(1-)

Chemical Property of (C₅(CH₃)5)Ru(CO)2(P(CH₃)2C₆H₅)⁽¹⁺⁾*I^(1-)=(C₅(CH₃)5)Ru(CO)2(P(CH₃)2C₆H₅)⁽¹⁺⁾I^(1-)

Chemical Property:

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Technology Process of (C₅(CH₃)5)Ru(CO)2(P(CH₃)2C₆H₅)⁽¹⁺⁾*I^(1-)=(C₅(CH₃)5)Ru(CO)2(P(CH₃)2C₆H₅)⁽¹⁺⁾I^(1-)

There total 2 articles about (C₅(CH₃)5)Ru(CO)2(P(CH₃)2C₆H₅)⁽¹⁺⁾*I^(1-)=(C₅(CH₃)5)Ru(CO)2(P(CH₃)2C₆H₅)⁽¹⁺⁾I^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

Cp*Ru(CO)2I + 2,2'-azobis(isobutyronitrile) (78-67-1) + Dimethyl(phenyl)phosphine (672-66-2) → (C5(CH3)5)Ru(CO)(P(CH3)2C6H5)I (103817-62-5) + (C5(CH3)5)Ru(CO)2(P(CH3)2C6H5)(1+)*I(1-)=(C5(CH3)5)Ru(CO)2(P(CH3)2C6H5)(1+)I(1-) (88296-33-7)

Guidance literature:

In toluene; heating (80°C, steam bath); pptn. of ((C5H5)Ru(CO)2(PMe2Ph))I, filtration, washing (hexane), evapn.of filtrate, chromy. (toluene, silica gel), crystn. of (C5H5)Ru(CO)(PMe2Ph)I; elem. anal.;

Reference yield:

iodo(cyclopentadienyl)dicarbonylruthenium(II) + (C5(CH3)5)Ru(CO)(P(CH3)2C6H5)CHO (88296-35-9) → dicarbonyl(cyclopentadienyl)hydridoruthenium + (η5-C5Me5)Ru(CO)2hydride (82728-97-0) + (C5(CH3)5)Ru(CO)(P(CH3)2C6H5)I (103817-62-5) + (C5(CH3)5)Ru(CO)2(P(CH3)2C6H5)(1+)*I(1-)=(C5(CH3)5)Ru(CO)2(P(CH3)2C6H5)(1+)I(1-) (88296-33-7)

Guidance literature:

In benzene; stirring (overnight), heating (65°C, 15 min); solvent removal (vac.); (1)H-NMR;

Reference yield:

(C5(CH3)5)Ru(CO)2(P(CH3)2C6H5)(1+)*I(1-)=(C5(CH3)5)Ru(CO)2(P(CH3)2C6H5)(1+)I(1-) (88296-33-7) → (C5(CH3)5)Ru(CO)(P(CH3)2C6H5)CHO (88296-35-9)

Guidance literature:

With {Ph₃PCuH}6; In tetrahydrofuran;

DOI:10.1021/ja00314a035

upstream raw materials:

(C₅(CH₃)5)Ru(CO)(P(CH₃)2C₆H₅)CHO

2,2'-azobis(isobutyronitrile)

Dimethyl(phenyl)phosphine

Downstream raw materials:

(C₅(CH₃)5)Ru(CO)(P(CH₃)2C₆H₅)CHO

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